2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Chemical Properties

Melting point:

204 °C

Boiling point:

641.3±57.0 °C(Predicted)

Density 

1.21±0.1 g/cm3(Predicted)

pka

0.92±0.10(Predicted)

form 

powder to crystal

color 

White to Almost white

Safety Information

HS Code 

2934.99.4400

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Usage And Synthesis

Uses

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and chemical production processes.

Synthesis

15.0 g of 2-(3-Bromophenyl)-4,6-diphenyl-l,3,5- triazine (32.4 mmol), 12.3 g of bis(pinacolato)diboron (48.6 mmol), 529 mg of Pd(dppf)Cl2.CH2Cl2 (0.647 mmol), 9.53 g of potassium acetate (97.1 mmol) and 323 ml of dioxane were put into a 1-neck round flask and reacted under reflux at 90° C. for 12 hours. After completion of the reaction, the solvent was removed under reduced pressure. The produced solid was dissolved in dichloromethane and then filtered through a Celite filter and washed with dichloromethane. The solvent was removed under reduced pressure and the resultant compound was crystallized with methanol to obtain 16.0 g of solid compound (intermediate 6) (yield: 96.8%).

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine(1269508-31-7)Related Product Information

• 2-(4-Biphenylyl)-4,6-dichloro-1,3,5-triazine
• 2,4-Dichloro-6-naphthalen-2-yl-[1,3,5]triazine
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