(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Chemical Properties

Melting point:

143°C (estimate)

Boiling point:

81 °C/16 mmHg (lit.)

Density 

0.899 g/mL at 25 °C (lit.)

refractive index 

n20/D 1.503

Flash point:

148 °F

storage temp. 

2-8°C

pka

8.88±0.50(Predicted)

form 

clear liquid

color 

Colorless to Light yellow to Light orange

optical activity

[α]20/D 49.2°, c = 1 in methanol

BRN 

3196218

CAS DataBase Reference

17279-31-1(CAS DataBase Reference)

Safety Information

Hazard Codes 

Xn

Risk Statements 

22-36

Safety Statements 

26

RIDADR 

2810

WGK Germany 

2

F 

8-10-23

HS Code 

2921490090

MSDS

• Language:English Provider:ACROS
• Language:English Provider:SigmaAldrich

(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Usage And Synthesis

Chemical Properties

clear colorless to yellow liquid

Purification Methods

The amine is mixed with aqueous 10N NaOH and extracted with toluene. The extract is washed with saturated aqueous NaCl, dried over K2CO3, and transferred to fresh K2CO3 until the solution is clear, and is filtered. The filtrate is distilled. If a short column packed with glass helices is used, the yield is reduced but a purer product is obtained. [Ingersoll Org Synth 25 89 1945, Snyder & Brewster J Am Chem Soc 71 291 4165 1949, Cope et al. J Am Chem Soc 71 3931 1949.] The (-)-picrate has m 140-141o from EtOH). The racemate [1126-71-2] has b 88-89o/16mm, 92-94o/30mm, 194-195o/760mm, d4 0.908. [Beilstein 13 III 2392.]

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