Ethyl 6,8-dichlorooctanoate Chemical Properties

Boiling point:

109 °C(Press: 0.7 Torr)

Density 

1.107 g/mL at 25 °C(lit.)

refractive index 

n20/D 1.462(lit.)

Flash point:

>230 °F

storage temp. 

Sealed in dry,Room Temperature

solubility 

Chloroform, Ethyl Acetate (Slightly)

form 

Oil

color 

Colourless to Pale Yellow

CAS DataBase Reference

1070-64-0(CAS DataBase Reference)

Safety Information

Hazard Codes 

Xi,N

Risk Statements 

36/37/38-51/53-43

Safety Statements 

26-36-61-37-24

RIDADR 

UN 3082 9 / PGIII

WGK Germany 

2

MSDS

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Ethyl 6,8-dichlorooctanoate Usage And Synthesis

Chemical Properties

Colourless to Pale Yellow Oil

Uses

6,8-Dichlorooctanoic Acid Ethyl Ester is an industrial toxin as well as an intermediate product of lipoic acid synthesis.

Flammability and Explosibility

Not classified

Synthesis

Dichloroethane in the organic solvent, 6-hydroxy -Chloro - octanoic acid ethyl ester with chlorinated reagent solid phosgene inN, N-dimethyl benzyl amine for the acid-binding agentEthyl 6-hydroxy-8-chlorooctanoate,Chlorination reagents,N, N-dimethylbenzylamine molar ratio1: 1.05: 0.12,The organic solvent was reacted with 6-hydroxy-8-The weight ratio of ethyl chlorocaprylate was1: 2.4 at a temperature ofN, N-dimethylbenzylamine was added dropwise at 10℃,Insulation temperature of 75 ,Insulation time 150min,In the reaction solution obtained,Water layer, water and 6 - hydroxy -8-chloro-ethyl octanoate weight ratio of 1:3, the upper organic phase.Vacuum distillation to collect vacuum 5mmHg,A temperature of 172-176℃,Ethyl 6,8-dichlorooctanoate,Product mol yield 95.68%, Purity 96.65%The bottom of the liquid base to adjust the pH value of 11,Layered,The upper layer was dewatered with sodium sulfateN, N-dimethylbenzylamine,The molar yield of the product was 96.69%Purity 99.71%.

Ethyl 6,8-dichlorooctanoate(1070-64-0)Related Product Information

• ISOXADIFEN-ETHYL
• Tris(trimethylsilyl)phosphate
• Ethanol
• Dichloroethane
• Sodium dichloroisocyanurate
• Ethyl caprylate
• Ethyl acetate
• Ethyl acetoacetate
• Dimethyl succinate
• Trinexapac-ethyl
• Thionyl chloride
• Ethyl formate
• Ethyl propionate
• Quinclorac
• Ethylparaben
• 2-Ethoxyethanol
• Diethyl ether
• 6,8-dichlorooctanoic acid