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3-Bromo-2-chlorophenol

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3-Bromo-2-chlorophenol Basic information

Product Name:
3-Bromo-2-chlorophenol
Synonyms:
  • 3-BROMO-2-CHLOROPHENOL
  • Phenol,3-bromo-2-chloro-
  • 3-Bromo-2-chlorophenol 98%
  • 3-Bromo
CAS:
863870-87-5
MF:
C6H4BrClO
MW:
207.45
Product Categories:
  • pharmacetical
Mol File:
863870-87-5.mol
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3-Bromo-2-chlorophenol Chemical Properties

Melting point:
60 °C
Boiling point:
246.1±20.0 °C(Predicted)
Density 
1.788±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
7.53±0.10(Predicted)
InChI
InChI=1S/C6H4BrClO/c7-4-2-1-3-5(9)6(4)8/h1-3,9H
InChIKey
DUKKNDLIWRYBCT-UHFFFAOYSA-N
SMILES
C1(O)=CC=CC(Br)=C1Cl
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Safety Information

HS Code 
2908190090
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3-Bromo-2-chlorophenol Usage And Synthesis

Synthesis

326.4 g (2.04 moles) of bromine is added dropwise in 6 hours with vigorous stirring, within a temperature range of between 20° and 45° C., to a mixture of 257.2 g (2 moles) of 2-chlorophenol, 1.0 g of zinc chloride and 1.0 g of diphenyl sulfide. After adding 70 ml of bromine, the temperature rises to 35° C. To avoid crystallization, the reaction mixture is afterwardheated to 40° C., Afterward, 20 ml of bromine is added dropwise. The remaining bromine is finally added at 45° C. After the addition of bromine is complete, stirring is maintained for 30 minutes at 50° C., and subsequently, the reaction product is freed at 60° C. under reduced pressure from dissolved hydrogen bromide to leave 414.5 g (99.8% of theory) of chlorobromophenol(3-Bromo-2-chlorophenol).

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