3-Bromo-2-chlorophenol
3-Bromo-2-chlorophenol Basic information
- Product Name:
- 3-Bromo-2-chlorophenol
- Synonyms:
-
- 3-BROMO-2-CHLOROPHENOL
- Phenol,3-bromo-2-chloro-
- 3-Bromo-2-chlorophenol 98%
- 3-Bromo
- CAS:
- 863870-87-5
- MF:
- C6H4BrClO
- MW:
- 207.45
- Product Categories:
-
- pharmacetical
- Mol File:
- 863870-87-5.mol
3-Bromo-2-chlorophenol Chemical Properties
- Melting point:
- 60 °C
- Boiling point:
- 246.1±20.0 °C(Predicted)
- Density
- 1.788±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 7.53±0.10(Predicted)
- InChI
- InChI=1S/C6H4BrClO/c7-4-2-1-3-5(9)6(4)8/h1-3,9H
- InChIKey
- DUKKNDLIWRYBCT-UHFFFAOYSA-N
- SMILES
- C1(O)=CC=CC(Br)=C1Cl
3-Bromo-2-chlorophenol Usage And Synthesis
Synthesis
326.4 g (2.04 moles) of bromine is added dropwise in 6 hours with vigorous stirring, within a temperature range of between 20° and 45° C., to a mixture of 257.2 g (2 moles) of 2-chlorophenol, 1.0 g of zinc chloride and 1.0 g of diphenyl sulfide. After adding 70 ml of bromine, the temperature rises to 35° C. To avoid crystallization, the reaction mixture is afterwardheated to 40° C., Afterward, 20 ml of bromine is added dropwise. The remaining bromine is finally added at 45° C. After the addition of bromine is complete, stirring is maintained for 30 minutes at 50° C., and subsequently, the reaction product is freed at 60° C. under reduced pressure from dissolved hydrogen bromide to leave 414.5 g (99.8% of theory) of chlorobromophenol(3-Bromo-2-chlorophenol).
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