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9-Phenyl-9H,9'H-[3,3']bicarbazolyl

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9-Phenyl-9H,9'H-[3,3']bicarbazolyl Basic information

Product Name:
9-Phenyl-9H,9'H-[3,3']bicarbazolyl
Synonyms:
  • 9-Phenyl-9H,9'H-[3,3']bicarbazolyl
  • 3-(9-Phenyl-9H-carbazol-3-yl)-9H-carbazole
  • 9-phenyl-9H,9'H-3,3'-bicarbazole
  • 3-(9-phenyl-carbazol-3-yl)-9H-carbazole
  • N-Phenyl-3,3'-bicarbazolyl
  • 3,3'-Bi-9H-carbazole, 9-phenyl-
  • 9-Phenyl-3,3'-bicarbazolyl
  • 9-phenyl-3,3'-bicarbazole
CAS:
1060735-14-9
MF:
C30H20N2
MW:
408.49
EINECS:
1312995-182-4
Mol File:
1060735-14-9.mol
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9-Phenyl-9H,9'H-[3,3']bicarbazolyl Chemical Properties

Boiling point:
685.6±37.0 °C(Predicted)
Density 
1.23±0.1 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
17.10±0.30(Predicted)
InChI
InChI=1S/C30H20N2/c1-2-8-22(9-3-1)32-29-13-7-5-11-24(29)26-19-21(15-17-30(26)32)20-14-16-28-25(18-20)23-10-4-6-12-27(23)31-28/h1-19,31H
InChIKey
GKTLHQFSIDFAJH-UHFFFAOYSA-N
SMILES
N1(C2=CC=CC=C2)C2=C(C=CC=C2)C2=C1C=CC(C1=CC3C4=C(NC=3C=C1)C=CC=C4)=C2
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Safety Information

HS Code 
2933998090
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9-Phenyl-9H,9'H-[3,3']bicarbazolyl Usage And Synthesis

Application

9-phenyl-3,3’-bicarbazolyl is the intermediate to synthesis electronic materials, such as OLED.9-phenyl-3,3’-bicarbazolyl is a kind of organic electroluminescent materials to make OLED display screen, and this intermediate can be used in OLED series, such as Thiophene series, Fluorene series, Boronic Acid series and so on.

Synthesis

A mixture of (9-phenyl-9H-carbazol-3-yl)boronic acid (14.2 g,49.5 mmol), 3-bromo-9H-carbazole (11.1 g, 45.0 mmol), Pd(PPh3)4(1.05 g, 0.9 mmol), K2CO3 (2.0 M aqueous solution, 80 mL), toluene(160 mL) and ethanol (80 mL) were stirred under nitrogen at 100 °Cfor 12 h. Until the reaction cooled to room temperature, the grey powder was filtered from the solution and was recrystallized by ethanol to afford 9-Phenyl-3,3'-bicarbazolyl (15.1 g, yield: 82 percent).

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