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1-bromodibenzo[b,d]furan

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1-bromodibenzo[b,d]furan Basic information

Product Name:
1-bromodibenzo[b,d]furan
Synonyms:
  • 1-Bromodibenzo[b,d]fur
  • 1-Brom-dibenzofuran
  • Dibenzofuran, 1-broMo-
  • 1-Bromodibenzofuran
  • 1-BroModibenzo[b,d]furan
  • -Bromodibenzo[b,d]furan
  • 1-BDPF
  • 1-bromo-dibenzofuran(1-BDPF)
CAS:
50548-45-3
MF:
C12H7BrO
MW:
247.09
Product Categories:
  • oled
Mol File:
50548-45-3.mol
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1-bromodibenzo[b,d]furan Chemical Properties

Melting point:
67℃
Boiling point:
343.8±15.0 °C(Predicted)
Density 
1.577±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Gray to Brown
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Safety Information

HS Code 
2932990090
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1-bromodibenzo[b,d]furan Usage And Synthesis

Uses

1-bromodibenzo[b,d]furan can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development and chemical and pharmaceutical production processes.

Synthesis


111 g (416 mmol) of 6?ˉ-bromo-2?ˉ-fluorobiphenyl-2-ol are dissolved in 21 of SeccoSolv DMF (max 0.003% of H20) and cooled to 5??C. 20 g (449 mmol) of sodium hydride (60% suspension in paraffin oil) are added in portions tothis solution, and the mixture is stirred for a further 20 mm. after the addition is complete and then heated at 100??C for 45 mm. After cooling, 500 ml of ethanol are slowly added to the mixture, which is then evaporated to dryness in a rotary evaporator and purified by chromatography. Yield: 90 g (367 mmol), 88.5% of theory.

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