2-Allyloxy-1,3,5-tribromobenzene
2-Allyloxy-1,3,5-tribromobenzene Basic information
- Product Name:
- 2-Allyloxy-1,3,5-tribromobenzene
- Synonyms:
-
- 1,3,5-tribromo-2-(2-propenyloxy)-benzen
- ALLYL 2,4,6-TRIBROMOPHENYL ETHER
- ALLYL TRIBROMOPHENYL ETHER
- Benzene,1,3,5-tribromo-2-(2-propenyloxy)
- TRIBROMOPHENYL ALLYL ETHER
- 2-allyloxy-1,3,5-tribromobenzene
- 1,3,5-TribroMo-2-(2-propen-1-yloxy)-benzene
- Allyl 2,4,6-tribromophenyl ether 98%
- CAS:
- 3278-89-5
- MF:
- C9H7Br3O
- MW:
- 370.86
- EINECS:
- 221-913-2
- Product Categories:
-
- Allyl Monomers
- Monomers
- Polymer Science
- Mol File:
- 3278-89-5.mol
2-Allyloxy-1,3,5-tribromobenzene Chemical Properties
- Melting point:
- 74-76 °C (lit.)
- Boiling point:
- 339.5±37.0 °C(Predicted)
- Density
- 1.950±0.06 g/cm3(Predicted)
- solubility
- Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
- form
- Solid
- color
- Off-White to Beige
- EPA Substance Registry System
- Allyl 2,4,6-tribromophenyl ether (3278-89-5)
MSDS
- Language:English Provider:SigmaAldrich
2-Allyloxy-1,3,5-tribromobenzene Usage And Synthesis
Application
1,3,5-Tribromo-2-(2-propen-1-yloxy)-benzene is used as a brominated flame retardant.
Not a dangerous good if item is equal to or less than 1g/ml and there is less than 100g/ml in the package.
Synthesis
To the ethanol solution of the sodium tribromophenolate salt prepared in the step 1), the dispersing agent sodium stearate 2.5 g is added.And catalyst II phenyl triethyl ammonium chloride 5.6g,The temperature is raised to 75 ?? C to reflux the reaction.Further, 1000 ml of an ethanol solution of chloropropene having a volume ratio of chloropropene to ethanol of 1:5 was slowly added thereto, and then the reaction was kept at 75 ?? C for 6.5 h until the end.Then, the temperature is lowered to 7 ?? C in sequence, and then suction filtration is performed to recover the ethanol solution.After washing the filter cake with water, the filter cake was dried at 60 ?? C.2,4,6-Tribromophenyl allyl ether was obtained as a white powdery solid in a yield of 96.2%.
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