4-METHOXY-3-NITROACETOPHENONE Chemical Properties

Melting point:

97-100 °C(lit.)

Boiling point:

315.1±22.0 °C(Predicted)

Density 

1.244±0.06 g/cm3(Predicted)

form 

powder to crystal

color 

White to Yellow to Green

BRN 

646069

CAS DataBase Reference

6277-38-9(CAS DataBase Reference)

Safety Information

Safety Statements 

22-24/25

WGK Germany 

3

HazardClass 

IRRITANT

HS Code 

2914790090

MSDS

• Language:English Provider:SigmaAldrich
• Language:English Provider:ALFA

4-METHOXY-3-NITROACETOPHENONE Usage And Synthesis

Uses

4′-Methoxy-3′-nitroacetophenone may be used to synthesize dimethylamino compound, via W₂ Raney nickel catalyzed reductive methylation.

Preparation

Preparation by reaction of acetyl chloride with 2-nitroanisole in the presence of aluminium chloride,
? in nitrobenzene at 0° ;
? in carbon disulfide.

General Description

4′-Methoxy-3′-nitroacetophenone can be synthesized from p-methoxyacetophenone via nitration.

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