2-(4-BROMOPHENOXY)ACETONITRILE Chemical Properties

Melting point:

52-54 °C

Boiling point:

303.1±17.0 °C(Predicted)

Density 

1.519±0.06 g/cm3(Predicted)

storage temp. 

Sealed in dry,2-8°C

form 

solid

color 

Brown

Safety Information

Hazard Codes 

Xn

Risk Statements 

22

RIDADR 

UN3439

WGK Germany 

3

HazardClass 

6.1

PackingGroup 

III

HS Code 

2926907090

MSDS

• Language:English Provider:ALFA

2-(4-BROMOPHENOXY)ACETONITRILE Usage And Synthesis

Synthesis

4-Bromophenol (10 g, 57.8 mmol), Cs2CO3 (24.48 g, 75.14 mmol) and chloroacetonitrile (5.66 g, 75.14 mmol) were dissolved in DMF. The mixture was then heated to 70°C for 5 hours, and transferred into a mixture of ice/H2O. The precipitate was filtered, and the resulting solid was partitioned between water and DCM. The aqueous phase was back extracted and the combined organic phases were washed with brine, dried over Na2SO4 and the solvent removed under reduced atmosphere, resulting a beige solid 2-(4-BROMOPHENOXY)ACETONITRILE. Yield: 12.18 g, 57.4 mmol (99% based on 4-bromophenol).

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