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9-Bromo-10-phenylanthracene

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9-Bromo-10-phenylanthracene Basic information

Product Name:
9-Bromo-10-phenylanthracene
Synonyms:
  • Anthracene, 9-Bromo-10-phenyl
  • 9-Bromo-10-phenylanthracene
  • 10-phenyl-9-BroMoanthracene
  • 9-Bromo-10-phenylant
  • 10-broMo-9-phenylanthracene
  • 9-bromo-10-phenylindole
  • 9-bromo-10-phenylanthrancene
  • 9-Bromo-10-phenyl
CAS:
23674-20-6
MF:
C20H13Br
MW:
333.22
EINECS:
621-755-8
Product Categories:
  • organic chemicals and derivatives/others
  • OLED
Mol File:
23674-20-6.mol
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9-Bromo-10-phenylanthracene Chemical Properties

Melting point:
154-155 °C
Boiling point:
449.7±14.0 °C(Predicted)
Density 
1.393
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Methanol (Slightly)
form 
Powder
color 
Pale yellow
Water Solubility 
Insoluble in water. Soluble in hot toluene, dimethylformamide.
InChIKey
WHGGVVHVBFMGSG-UHFFFAOYSA-N
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Safety Information

Safety Statements 
24/25
HS Code 
29039990
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9-Bromo-10-phenylanthracene Usage And Synthesis

Description

9-Bromo-10-phenylanthracene is a yellow-white solid powder that is commonly used as an organic synthesis intermediate.It is not soluble in water but can dissolve in dimethyl sulfoxide, N,N-dimethylformamide, and other polar solvents. It is also soluble in hot non-polar solvents due to its low polarity.

Chemical Properties

Pale yellow powder

Uses

It is used as an OLED material.

Uses

9-Bromo-10-phenylanthracene is an anthracene compound for proteomics research.

Preparation

9-Phenylanthracene (2.5g, 9.83mmol) and NBS (2.1g, 11.8mmol) were dissolved in 80mL CHCl3. Then the mixture was heated to 60°C for 2h under N2. After cooled to room temperature, 20 mL water was added. And the mixture was extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation.The crude product was recrystallized from methanol to get a green-yellow powder (2g, 61.2%). 1H NMR (500 MHz, CDCl3) δ 8.67 – 8.61 (m, 2H), 7.71 – 7.65 (m, 2H), 7.64 – 7.56 (m, 5H), 7.45 – 7.37 (m, 4H). EI-MS (m/z): Calculated for C20H13Br: 333.22. Found [M+]: 332.30.

Synthesis of 9-bromo-10-phenylanthracene

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