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2,4,6-triiodoaniline

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2,4,6-triiodoaniline Basic information

Product Name:
2,4,6-triiodoaniline
Synonyms:
  • 2,4,6-triiodoaniline
MF:
C6H4I3N
MW:
470.81607
Mol File:
Mol File
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2,4,6-triiodoaniline Usage And Synthesis

Synthesis

2,4,6-Triiodoaniline was prepared analogously to 2,4-Diiodoaniline with the use of 3 equiv. of KICl2. The mixture of aniline and HCl was diluted to 0.75 L. The yield of triiodoaniline was 4.51 g (87%), m.p. 185 °C (cf. lit. data2: m.p. 185 °C). 1H NMR (CDCl3), δ: 4.63 (br.s, 2 H, NH2); 7.85 (s, 2 H, ArH).

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