CYCLODECANONE Chemical Properties

Melting point:

21-24 °C (lit.)

Boiling point:

106-107 °C/12 mmHg (lit.)

Density 

0.958 g/mL at 25 °C (lit.)

refractive index 

n20/D 1.482(lit.)

Flash point:

180 °F

storage temp. 

2-8°C

solubility 

Chloroform (Slightly), Methanol (Slightly)

form 

Colourless Oil to Semi-Solid

BRN 

1617127

LogP

2.929 (est)

Safety Information

Hazard Codes 

Xi

Risk Statements 

36

Safety Statements 

26

WGK Germany 

3

F 

9-23

HS Code 

29142990

MSDS

• Language:English Provider:SigmaAldrich

CYCLODECANONE Usage And Synthesis

Chemical Properties

White solid or colorless liquid

Synthesis Reference(s)

Journal of the American Chemical Society, 86, p. 3068, 1964 DOI: 10.1021/ja01069a019
Organic Syntheses, Coll. Vol. 4, p. 218, 1963
Synthetic Communications, 9, p. 437, 1979 DOI: 10.1080/00397917908064174

Purification Methods

Purify the ketone via the semicarbazone (m 205-207o, from EtOH) and distil it through an efficient column. It sublimes in a vacuum. The oxime has m 80o, from MeOH or by sublimation in a high vacuum. [Cope et al. Org Synth Coll Vol IV 218 1963, Prelog et al. Helv Chim Acta 30 1746 1947, Ruzicka et al. Helv Chim Acta 11 675 1930, Beilstein 7 III 134, 7 IV 76.]

CYCLODECANONE(1502-06-3)Related Product Information

• Prednisone
• 5ALPHA-ANDROST-16-EN-3-ONE
• FRIEDELIN
• 11-DEHYDROCORTICOSTERONE
• Cortisone acetate
• Stanolone
• HECOGENIN ACETATE
• 1-DECALONE
• CORTISONE
• Mestanolone
• Androstanolone 17-benzoate
• Adrenosterone
• CYCLODECANONE
• 11-KETOANDROSTERONE
• 1-DEHYDROANDRENOSTERONE
• 5B-ANDROSTANE-3,17-DIONE
• 3alpha,17,21-trihydroxy-5beta-pregnane-11,20-dione 21-acetate
• 11-DEHYDROCORTICOSTERONE ACETATE