5-Bromo-3-pyridinemethanol Chemical Properties

Boiling point:

291.5±25.0 °C(Predicted)

Density 

1.67

refractive index 

1.5940-1.5980

storage temp. 

Keep in dark place,Inert atmosphere,Room temperature

pka

13.29±0.10(Predicted)

form 

Liquid or Low Melting Solid

color 

Clear pale yellow

InChIKey

WDVDHJLKXYCOFS-UHFFFAOYSA-N

Safety Information

Hazard Codes 

Xi

Hazard Note 

Irritant

HS Code 

2933399990

5-Bromo-3-pyridinemethanol Usage And Synthesis

Synthesis

Sodium borohydride (2.2 g, 59.1 mmol) was added to a suspension of 5-bromo-pyridine-3-carbaldehyde (10.0 g, 53.7 mmol) in MeOH (100 mL) at 0° C. The mixture was stirred at 0° C. for 1 hour before it was quenched by adding water (5.0 mL). Evaporation of solvents afforded a light yellowish oil, which was re-dissolved in EtOAc and washed with water. The organic layer was dried over anhy. Na2SO4, filtered and concentrated in vacuo to give 5-Bromo-3-pyridinemethanol (9.6 g, 95 per cent) as a colourless oil.

5-Bromo-3-pyridinemethanol(37669-64-0)Related Product Information

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• 2-(3-bromopyridin-4-yl)ethanol
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• 5,6-DIBROMOPYRIDINE-3-CARBOXYLIC ACID
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• Methyl 5-bromo-2-chloropyridine-3-carboxylate
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• Methyl 5-bromonicotinate
• Ethyl 5-bromonicotinate
• 5-Bromo-2-hydroxymethylpyridine
• 5-Bromopyridine-2-methanol
• (2-BROMO-PYRIDIN-4-YL)-METHANOL
• (6-BROMO-PYRIDIN-2-YL)-METHANOL,(6-Bromo-pyridin-2-yl)-methanol >97%
• (2-AMINO-5-BROMO-PYRIDIN-3-YL)-METHANOL
• (2-BROMO-PYRIDIN-5-YL)-METHANOL,(6-BROMO-PYRIDIN-3-YL)-METHANOL
• 3-Pyridinemethanol