Bromotriphenylethylene
Bromotriphenylethylene Basic information
- Product Name:
- Bromotriphenylethylene
- Synonyms:
-
- bromotriphenyl-ethylen
- 1-bromo-1,2,2-triphenylethylene
- 2-BROMO-1,1,2-TRIPHENYLETHYLENE
- AURORA KA-6594
- BROMOTRIPHENYLETHYLENE
- Benzene, 1,1,1-(1-bromo-1-ethenyl-2-ylidene)tris-
- à-bromo-à'-phenylstilbene
- triphenylvinyl bromide
- CAS:
- 1607-57-4
- MF:
- C20H15Br
- MW:
- 335.24
- EINECS:
- 216-531-8
- Product Categories:
-
- Pharmaceutical Intermediates
- Mol File:
- 1607-57-4.mol
Bromotriphenylethylene Chemical Properties
- Melting point:
- 115-117 °C(lit.)
- Boiling point:
- 391.41°C (rough estimate)
- Density
- 1.3419 (rough estimate)
- refractive index
- 1.6000 (estimate)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder to crystal
- color
- Light orange to Yellow to Green
- BRN
- 2052962
- CAS DataBase Reference
- 1607-57-4(CAS DataBase Reference)
Safety Information
- Safety Statements
- 24/25
- WGK Germany
- 3
- RTECS
- KU8850000
- HS Code
- 29036990
MSDS
- Language:English Provider:1-Bromo-1,2,2-triphenylethylene
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
- Language:English Provider:ALFA
Bromotriphenylethylene Usage And Synthesis
Chemical Properties
light yellow crystalline powder
Synthesis
58-72-0
1607-57-4
GENERAL METHOD: Tristyrene (1.0 g, 3.49 mmol) was dissolved in chloroform (15 mL) and a chloroform (10 mL) solution of bromine (0.49 g, 3.06 mmol) was added slowly and dropwise. Upon completion of the reaction, the reaction mixture was decanted and the solvent was subsequently removed by distillation. The residue was recrystallized twice from ethanol to give triphenylene bromide (0.8 g, 62%) as colorless needle-like crystals.
References
[1] Bulletin of the Chemical Society of Japan, 1988, vol. 61, p. 449 - 454
[2] Chemische Berichte, 1987, vol. 120, p. 1897 - 1904
[3] Tetrahedron, 2012, vol. 68, # 36, p. 7309 - 7316
[4] Journal of the Chemical Society, 1933, p. 69,74
[5] Journal of the American Chemical Society, 1932, vol. 54, p. 2049,2051
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Bromotriphenylethylene(1607-57-4)Related Product Information
- Polyethylene
- Benzyldodecyldimethylammonium bromide
- Decabromodiphenyl Ethane
- Triphenylethylene
- Vinyl bromide
- Styrene
- 1,2-DIBROMOETHYLENE
- ETHYLENE
- Benzbromarone
- TRIPHENYLFLUOROSILANE
- beta-Bromostyrene
- 2-Methyl-2-butene
- CIS-BETA-METHYLSTYRENE
- 2-Phenyl-1-propene
- CIS-2-BUTENE
- 2-PHENYL-2-BUTENE
- 1,1-Diphenylethylene
- Bromine