Cyclohexylhydrazine hydrochloride Chemical Properties

Melting point:

110-114 °C(lit.)

storage temp. 

under inert gas (nitrogen or Argon) at 2–8 °C

form 

Crystalline Powder

color 

White

Water Solubility 

almost transparency

InChI

InChI=1S/C6H14N2.ClH/c7-8-6-4-2-1-3-5-6;/h6,8H,1-5,7H2;1H

InChIKey

JZRHODNPRNTXKO-UHFFFAOYSA-N

SMILES

C1(NN)CCCCC1.Cl

CAS DataBase Reference

24214-73-1(CAS DataBase Reference)

Safety Information

Hazard Codes 

C

Risk Statements 

34

Safety Statements 

26-36/37/39-45

RIDADR 

UN 3263 8/PG 2

WGK Germany 

3

HazardClass 

8

PackingGroup 

Ⅱ

HS Code 

29280000

MSDS

• Language:English Provider:SigmaAldrich

Cyclohexylhydrazine hydrochloride Usage And Synthesis

Chemical Properties

White to light yellow powder,crystals or

Synthesis

GENERAL METHOD: tert-Butyl 2-cyclohexylhydrazine-1-carboxylate (1.9 g, 8.87 mmol) was dissolved in dioxane and to this solution was added a dioxane solution (20 mL) of 4 M HCl. The reaction mixture was heated to reflux and stirred overnight. Upon completion of the reaction, it was cooled to room temperature, the precipitated white precipitate was collected by filtration, washed with a small amount of cold dioxane and dried to give cyclohexylhydrazine hydrochloride (1.8 g, yield: >100%) as a white solid.

References

[1] Patent: WO2016/123392, 2016, A2. Location in patent: Paragraph 00476
[2] Patent: WO2014/82598, 2014, A1. Location in patent: Paragraph 0419
[3] Journal of Organic Chemistry, 1981, vol. 46, # 26, p. 5413 - 5414
[4] Patent: WO2005/40169, 2005, A2. Location in patent: Page/Page column 150

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