2,4-Dichloro-6-phenyl-1,3,5-triazine Chemical Properties

Melting point:

gt. 119.0 to 123.0 °C

Boiling point:

136°C/1mmHg(lit.)

Density 

1.428±0.06 g/cm3(Predicted)

storage temp. 

Keep in dark place,Sealed in dry,Room Temperature

form 

powder to crystal

pka

-1.67±0.10(Predicted)

color 

White to Orange to Green

InChI

InChI=1S/C9H5Cl2N3/c10-8-12-7(13-9(11)14-8)6-4-2-1-3-5-6/h1-5H

InChIKey

AMEVJOWOWQPPJQ-UHFFFAOYSA-N

SMILES

N1=C(C2=CC=CC=C2)N=C(Cl)N=C1Cl

CAS DataBase Reference

1700-02-3(CAS DataBase Reference)

Safety Information

HS Code 

2933998090

2,4-Dichloro-6-phenyl-1,3,5-triazine Usage And Synthesis

Description

2,4-Dichloro-6-phenyl-1,3,5-triazine is a heterocyclic derivative and can be used as intermediate of synthetic materials.

Chemical Properties

White to Orange to Green powder to crystal.

Uses

2,4-Dichloro-6-phenyl-1,3,5-triazine, is a building block as an OLED intermediate for the synthesis of bipolar host materials such as 2,4,6-tris(4-(N,N-diphenylamino)phenyl)-1,3,5-triazine (TDPA–TRZ) for phosphorescent organic light-emitting diodes (PhOLED).

Synthesis

2,4-Dichloro-6-phenyl-1,3,5-triazine was prepared by reaction of 36.2 g (0.21 mol) of 2,4-dihydroxy-6-phenyl-1 ,3,5-triazine with 180 g (1.51 mol) of thionyl chloride and 17.3 g of N,N-dimethylformamide (DMF) at 60°C for 3 h. The excess thionyl chloride was distilled,and the residue was poured into water to give a product.The white product was filtered off, dried, and recrys-tallized from benzene to give a yield of 22.0 g (47.4%).

2,4-Dichloro-6-phenyl-1,3,5-triazine(1700-02-3)Related Product Information

• Tris(triphenylphosphine)rhodiu
• Triphenylphosphine oxide
• 1,3,5-Triazine
• Dichloromethylphenylsilane
• Dichloroacetic acid
• Phenylphosphonic dichloride
• Triphenylmethyl Chloride
• Triphenyltin acetate
• PHENYL VALERATE
• 2,3,5-Triphenyltetrazolium chloride
• Triphenylphosphine
• Diphenyl ether
• PHENYL RESIN
• Phenylacetic acid
• 2,4-Dichloro-1,3,5-triazine
• 1,3,5-Triazine, 2-phenyl- (9CI)
• 1-(4-AMINO-3-CHLORO-PHENYL)-ETHANONE
• 1-(4,6-DICHLORO-1,3,5-TRIAZIN-2-YL)PYRENE