Basic information Safety Supplier Related

pelletierine

Basic information Safety Supplier Related

pelletierine Basic information

Product Name:
pelletierine
Synonyms:
  • 1-piperidin-2-ylacetone
  • pelletierine
  • 2-Acetonylpiperidinepunicineisopelletierine, (.+/-.)-pelletierine
  • isopelletierine
  • 1-(2-Piperidinyl)-2-propanone
  • 1-(2-Piperidyl)-2-propanone
  • 2-(2-Oxopropyl)piperidine
  • 1-piperidin-2-ylpropan-2-one
CAS:
4396-01-4
MF:
C8H15NO
MW:
141.21
EINECS:
224-523-0
Mol File:
4396-01-4.mol
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pelletierine Chemical Properties

Melting point:
130-132 °C
Boiling point:
195 °C
Density 
0.918±0.06 g/cm3(Predicted)
storage temp. 
Hygroscopic, -20°C Freezer, Under inert atmosphere
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly)
form 
Oil
pka
pK1:9.45 (15°C)
color 
Colourless to Light Yellow
Stability:
Hygroscopic
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pelletierine Usage And Synthesis

Description

An alkaloid of this name was discovered by Tanret but when this alkaloid was shown to be (±)-pelletierine, the name was adopted for this particular base isolated from Punica granatum. The alkaloid is an oily liquid which yields a number of well crystalline salts and derivative: the hydrochloride, m.p. 143°C; hydrobromide, m.p. 149°C; picrate, m.p. 147 -8°C and the picrolonate, m.p. 185-6°C. The N-acetyl derivative is an oily liquid, b.p. 110-5°C/0.I mm while the N-benzoyl compound is crystalline with m.p. 72-4°C. The alkaloid may be prepared by the demethylation of methylisopelletierine, the action being revers_x0002_ible.

Definition

ChEBI: Pelletierine is a citraconoyl group.

References

Tanret., Compt. rend., 88, 716 (1879) Tanret., ibid, 90, 696 (1880) Hesse., Rev. trav. Chim., 52, 1005 (1919) Hess, Littman., Annalen, 494, 7 (1932) Wibaut, Kloppenburg, Beets., Rev. trav. Chim., 63, 134 (1944) Anet, Hughes, Ritchie., Nature, 164, 50 I (1949) Galinovsky, Branchetti, Vogl.,Monatsh., 84, 1221 (1953) Galinovsky, Hollinger., ibid, 85, 1012 (1954) Wibaut, Hirschel., Rev. trav. Chim., 75,225 (1956)

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