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3-Nitrobenzaldehyde

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3-Nitrobenzaldehyde Basic information

Product Name:
3-Nitrobenzaldehyde
Synonyms:
  • M-Nitrobenzldehyde
  • 3-Nitrobenzaldehyde99%
  • 3-NITRO BENZALDEHYDE GR
  • 3-NITROBENZALDEHYDE / M-NITROBENZALDEHYDE
  • m-NITROBENZALDEHYDE pure
  • 3-Nitrobenzaldehyde ,98%
  • 3-Nitrobenzaldehyde, 99% 100GR
  • 3-NITROBENZALDEHYDE FOR SYNTHESIS
CAS:
99-61-6
MF:
C7H5NO3
MW:
151.12
EINECS:
202-772-6
Product Categories:
  • Pharmaceutical intermediates
  • Nicardipine
  • Aldehydes
  • C7
  • Carbonyl Compounds
  • Aromatic Aldehydes & Derivatives (substituted)
  • Benzaldehyde
Mol File:
99-61-6.mol
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3-Nitrobenzaldehyde Chemical Properties

Melting point:
56 °C
Boiling point:
285-290 °C
Density 
1.2792
vapor density 
5.21 (vs air)
refractive index 
1.5800 (estimate)
Flash point:
164°C/23mm
storage temp. 
?20°C
solubility 
1.6g/l
form 
Granular Powder
color 
Yellow to yellow-brown
Water Solubility 
Slightly soluble in water.
Sensitive 
Air Sensitive
Merck 
14,6587
BRN 
386795
CAS DataBase Reference
99-61-6(CAS DataBase Reference)
NIST Chemistry Reference
Benzaldehyde, 3-nitro-(99-61-6)
EPA Substance Registry System
Benzaldehyde, 3-nitro- (99-61-6)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38-51/53-22
Safety Statements 
26-36-24/25-61-37/39-29
WGK Germany 
3
RTECS 
CU7250000
Hazard Note 
Irritant
TSCA 
Yes
HS Code 
29130000
Toxicity
LD50 orally in Rabbit: 1075 mg/kg

MSDS

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3-Nitrobenzaldehyde Usage And Synthesis

Chemical Properties

yellowish to yellow-brown granular powder

Uses

3-Nitrobenzaldehyde is a benzaldhyde with a nitro group in the meta position.

Synthesis Reference(s)

Organic Syntheses, Coll. Vol. 3, p. 644, 1955
Tetrahedron Letters, 28, p. 1195, 1987 DOI: 10.1016/S0040-4039(00)95324-3

Purification Methods

Crystallise the aldehyde from water or EtOH/water, then sublime it twice at 2mm pressure at a temperature slightly above its melting point. [Beilstein 7 IV 591.]

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