5,7-Dihydro-indolo[2,3-b]carbazole
5,7-Dihydro-indolo[2,3-b]carbazole Basic information
- Product Name:
- 5,7-Dihydro-indolo[2,3-b]carbazole
- Synonyms:
-
- 5,7-DIHYDRO-INDOLO[2,3-B]CARBAZOLE
- 5H,7H-indolo[2,3-b]carbazole
- 5,7-Dihydro-indolo[2,3-b]carbazole (DHIC)
- Indolo[2,3-b]carbazole, 5,7-dihydro-
- 5,7-Dihydroindolo[2,3-b]carbazole,96%
- 1,3-Dihydroindolo[2,3-b ]carbazole
- CAS:
- 111296-90-3
- MF:
- C18H12N2
- MW:
- 256.3
- Product Categories:
-
- OLED
- Mol File:
- 111296-90-3.mol
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5,7-Dihydro-indolo[2,3-b]carbazole Chemical Properties
- Melting point:
- 348-360℃
- Boiling point:
- 569.8±23.0 °C(Predicted)
- Density
- 1.404±0.06 g/cm3 (20 ºC 760 Torr)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 16.70±0.30(Predicted)
- form
- Solid
- color
- Pale brown to brown
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5,7-Dihydro-indolo[2,3-b]carbazole Usage And Synthesis
Uses
5,7-Dihydro-indolo[2,3-b]carbazole could be a useful thermally activated delayed fluorescence (TADF) emitter for making efficient OLEDs.
Synthesis
4′,6′-Dinitro-1,1′:3′,1′′-terphenyl 27.5 g (86 mmol) in a 1 L reactor,57.8 g (348 mmol) of triphenylphosphine,300 mL of dichlorobenzene was added and the mixture was stirred under reflux for 3 days. After completion of the reaction, dichlorobenzene was removed, and the residue was separated by column chromatography to obtain 10.8 g 5,7-Dihydro-indolo[2,3-b]carbazole (Yield 49.0%)
5,7-Dihydro-indolo[2,3-b]carbazoleSupplier
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