ANTHRACENE, 9-BROMO-10-(1-NAPHTHALENYL)- Chemical Properties

Melting point:

177.0 to 181.0 °C

Boiling point:

508.0±19.0 °C(Predicted)

Density 

1.402±0.06 g/cm3(Predicted)

storage temp. 

Sealed in dry,Room Temperature

solubility 

soluble in Toluene

form 

Solid

color 

Pale yellow

InChI

InChI=1S/C24H15Br/c25-24-21-13-5-3-11-19(21)23(20-12-4-6-14-22(20)24)18-15-7-9-16-8-1-2-10-17(16)18/h1-15H

InChIKey

SYACRXBYRNYMLN-UHFFFAOYSA-N

SMILES

C1=C2C(C(C3=C4C(C=CC=C4)=CC=C3)=C3C(=C2Br)C=CC=C3)=CC=C1

Safety Information

HS Code 

2903.99.8001

ANTHRACENE, 9-BROMO-10-(1-NAPHTHALENYL)- Usage And Synthesis

Uses

9-Bromo-10-(1-Naphthyl)anthracene is an intermediate in organic synthesis and chemical and pharmaceutical research and development. It is mainly used as an OLED intermediate in laboratory research and development and chemical and pharmaceutical production.

Application

9-Bromo-10-(1-Naphthyl)anthracene is a heterocyclic organic compound that can be used as a pharmaceutical intermediate.

Chemical Properties

Off-white powder

Synthesis

The general procedure for the synthesis of 9-bromo-10-(1-naphthalenyl)anthracene using 9-(naphthalen-1-yl)anthracene as starting material was as follows: 9-(naphthalen-1-yl)anthracene (88 g, 0.29 mol) was dissolved in dimethylformamide (700 mL) in a 2 L four-necked round-bottomed flask. Subsequently, a solution of N-bromosuccinimide (NBS, 70.7 g, 0.4 mol) in dimethylformamide (200 mL) was added slowly and dropwise. The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the reaction mixture was poured into water to precipitate 9-bromo-10-(1-naphthyl)anthracene (108 g, 97.5% yield).

References

[1] Journal of Materials Chemistry, 2012, vol. 22, # 1, p. 123 - 129
[2] Patent: US2017/12214, 2017, A1. Location in patent: Paragraph 0166; 0167
[3] Chemical Communications, 2016, vol. 52, # 73, p. 10956 - 10959
[4] Patent: KR2016/90242, 2016, A. Location in patent: Paragraph 0266; 0267; 0268; 0269; 0270; 0271
[5] Patent: KR2017/55704, 2017, A. Location in patent: Paragraph 0111; 0118-0123

ANTHRACENE, 9-BROMO-10-(1-NAPHTHALENYL)-(400607-04-7)Related Product Information

• 3-bromo-9-phenyl-9H-carbazole
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