1,2-bis(4-hydroxyphenyl)ethan-1-one
1,2-bis(4-hydroxyphenyl)ethan-1-one Basic information
- Product Name:
- 1,2-bis(4-hydroxyphenyl)ethan-1-one
- Synonyms:
-
- 1,2-bis(4-hydroxyphenyl)ethan-1-one
- Ethanone, 1,2-bis(4-hydroxyphenyl)-
- CAS:
- 3669-47-4
- MF:
- C14H12O3
- MW:
- 228.24
- Mol File:
- 3669-47-4.mol
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1,2-bis(4-hydroxyphenyl)ethan-1-one Chemical Properties
- Melting point:
- 215–219°C
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1,2-bis(4-hydroxyphenyl)ethan-1-one Usage And Synthesis
Preparation
Preparation by total demethylation of 4-methoxyphenyl 4-methoxybenzyl ketone (4,4′-dimethoxydeoxybenzoin),
? with refluxing pyridinium chloride (4 equiv) for 1 h (80–85%);
? with boiling a mixture of 50% aqueous hydriodic acid and phenol for 30 min (94%);
? with hydriodic acid (d = 1.7) in acetic acid at 135–140° for 10 min (quantitative yield);
? with aluminium chloride in refluxing benzene for 1.5 h (25%).
1,2-bis(4-hydroxyphenyl)ethan-1-oneSupplier
AstaTech (Chengdu) Pharma. Co., Ltd.
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SanoChem (Chengdu) Tech. Co., Ltd.
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