3-AMINOBENZOYLMETHYLAMIDE Chemical Properties

Melting point:

119°C

Boiling point:

346.7±25.0 °C(Predicted)

Density 

1.137±0.06 g/cm3(Predicted)

storage temp. 

Keep in dark place,Sealed in dry,Room Temperature

form 

powder to crystaline

pka

15.19±0.46(Predicted)

color 

White to Light yellow to Light red

CAS DataBase Reference

25900-61-2(CAS DataBase Reference)

Safety Information

Hazard Codes 

Xi,Xn

Risk Statements 

36/37/38-43-22

Safety Statements 

26-36/37/39-36/37

WGK Germany 

3

HS Code 

2924.29.7790

HazardClass 

IRRITANT

3-AMINOBENZOYLMETHYLAMIDE Usage And Synthesis

Synthesis

General procedure for the synthesis of 3-amino-N-methylbenzamide from N-methyl-3-nitrobenzamide: A mixture of N-methyl-3-nitrobenzamide (2.47 g, 13.71 mmol) with 10% Pd/C catalyst (0.5 g) in methanol (50 mL) was subjected to hydrogenation at room temperature and atmospheric pressure overnight. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was subsequently concentrated. The resulting crude product was used directly in the subsequent reaction steps without further purification. (Yield: 2.06 g, 100%)

References

[1] Patent: US2004/97493, 2004, A1. Location in patent: Page/Page column 24
[2] Patent: US2010/160323, 2010, A1. Location in patent: Page/Page column 54
[3] Journal of Chemical Research, 2006, # 4, p. 223 - 224
[4] Patent: US5589489, 1996, A
[5] Patent: EP2774918, 2014, A1. Location in patent: Paragraph 0126; 0133

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