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3-Ethynylthiophene

Basic information Uses Safety Supplier Related

3-Ethynylthiophene Basic information

Product Name:
3-Ethynylthiophene
Synonyms:
  • 3-ETHYNYLTHIOPHENE 96
  • thienylacetylene
  • Thiophene, 3-ethynyl- (9CI)
  • 3-Ethynylthiophene
  • (Thien-3-yl)acetylene
  • 3-Thienylacethylene
  • Thiophene, 3-ethynyl-
  • 3-Ethynylthiophene 96%
CAS:
67237-53-0
MF:
C6H4S
MW:
108.16
Product Categories:
  • Building Blocks
  • Heterocyclic Building Blocks
  • Heterocyclic Compounds
  • Thiophenes
Mol File:
67237-53-0.mol
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3-Ethynylthiophene Chemical Properties

Boiling point:
152-153 °C (lit.)
Density 
1.098 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.5800(lit.)
Flash point:
115 °F
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
form 
Liquid
color 
Colorless to yellow to orange
Water Solubility 
Slightly soluble in water.
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Safety Information

Hazard Codes 
Xi
Risk Statements 
10-37/38-41
Safety Statements 
16-26-39
RIDADR 
UN 1993 3/PG 3
WGK Germany 
3
HazardClass 
3
PackingGroup 
III
HS Code 
29349990
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3-Ethynylthiophene Usage And Synthesis

Uses

3-Ethynylthiophene is used in preparation of benzothiazonines by rhodium-catalyzed denitrogenative annulation reactions of sulfonylaryltriazoles with thiochromones.

Uses

3-Ethynylthiophene may be used in the synthesis of the following:

  • 1-(2-bromobenzyl)-4-(thiophen-3-yl)-1H-1,2,3-triazole which is obtained by heating with 2-iodophenylethylazide in the presence of copper acetate monohydrate catalyst in N-methyl-2-pyrrolidone
  • N-benzyl-1-phenyl-5-(thiophen-3-yl)-4-pentyn-2-amine via a multi-step reaction process
  • [(C4H3S-3)C≡CAg]n, a polymeric compound obtained via reaction with silver nitrate in the presence of triethylamine in acetonitrile
  • 4,5-bis(thiophen-3-ylethynyl)phthalonitrile via Sonogashira cross-coupling reaction with 4,5-dichlorophthalonitrile

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