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4-Bromo-2,6-dichlorophenol

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4-Bromo-2,6-dichlorophenol Basic information

Product Name:
4-Bromo-2,6-dichlorophenol
Synonyms:
  • 2,6-Dichloro-4-bromophenol
  • 3-(1,2,3,4-tetrazol-1-yl)benzoic acid
  • 3-(1-tetrazolyl)benzoic acid
  • 4-Bromo-2,6-dichlorophenol, >=97%
  • Phenol, 4-bromo-2,6-dichloro-
  • 4-BROMO-2,6-DICHLOROPHENOL
CAS:
3217-15-0
MF:
C6H3BrCl2O
MW:
241.9
EINECS:
221-740-2
Product Categories:
  • Phenol&Thiophenol&Mercaptan
Mol File:
3217-15-0.mol
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4-Bromo-2,6-dichlorophenol Chemical Properties

Melting point:
64-65℃
Boiling point:
247℃
Density 
1.890
Flash point:
103℃
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
Powder
pka
6.46±0.23(Predicted)
color 
Off-white
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Safety Information

HazardClass 
IRRITANT
HazardClass 
6.1
HS Code 
2908190090
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4-Bromo-2,6-dichlorophenol Usage And Synthesis

Synthesis

Obtained by bromination and chlorination of o-chlorophenol: dissolve o-chlorophenol in carbon tetrachloride, add bromine dropwise with stirring at below 30°C, continue stirring and react for 2h after addition, then remove hydrobromic acid at room temperature, recover carbon tetrachloride and distill under reduced pressure, collect the fraction of 110-120°C (2kPChemicalbooka), and obtain 4-bromo-2-chlorophenol. Dissolve 4-bromo-2-chlorophenol in acetic acid and pass chlorine gas under ice-cold conditions until no more crystals are precipitated. Heat and reflux until all crystals are dissolved, decolorized, filtered, cool and crystallized, filter, and wash with petroleum ether to obtain the finished product 4-Bromo-2,6-dichlorophenol.

4-Bromo-2,6-dichlorophenol Preparation Products And Raw materials

Raw materials

4-Bromo-2,6-dichlorophenolSupplier

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