Basic information Safety Supplier Related

DL-CAMPHORIC ANHYDRIDE

Basic information Safety Supplier Related

DL-CAMPHORIC ANHYDRIDE Basic information

Product Name:
DL-CAMPHORIC ANHYDRIDE
Synonyms:
  • (+/-)-1,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE
  • 1,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE
  • DL-CAMPHORIC ANHYDRIDE
  • DL-CAMPHOR ANHYDRIDE
  • (+/-)-CAMPHORIC ACID ANHYDRIDE
  • (+/-)-CAMPHORIC ANHYDRIDE
  • (±)-Camphoricanhydride,98%
  • DL-Camphoric anhydride,98%
CAS:
595-30-2
MF:
C10H14O3
MW:
182.22
EINECS:
209-861-9
Product Categories:
  • FINE Chemical & INTERMEDIATES
Mol File:
595-30-2.mol
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DL-CAMPHORIC ANHYDRIDE Chemical Properties

Melting point:
222-225 °C
Boiling point:
270 °C
Density 
1.1940
refractive index 
1.5320 (estimate)
storage temp. 
2-8°C
Water Solubility 
Hydrolyzes in water.
Sensitive 
Moisture Sensitive
CAS DataBase Reference
595-30-2(CAS DataBase Reference)
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Safety Information

Hazard Codes 
Xn
Risk Statements 
22-36/37/38
Safety Statements 
26
WGK Germany 
3
10-21

MSDS

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DL-CAMPHORIC ANHYDRIDE Usage And Synthesis

Chemical Properties

white fine crystalline powder

Uses

(+/-)-Camphoric anhydride is useful in the synthesis of aliphatic-aromatic copolyesters. It is also used as pharmaceutical intermediates.

Purification Methods

Crystallise the anhydride from EtOH. If it contains too much of the acid (by IR), then reflux it in Ac2O, concentrate and collect the crystals, wash them with pet ether and dry them. [Bunton et al J Chem Soc 2918 1963, NMR: Baker & Davis Tetrahedron 24 1663 1968, Beilstein 18 H 400, 401.]

DL-CAMPHORIC ANHYDRIDESupplier

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