DI-TERT-BUTYL HYDRAZODICARBOXYLATE Chemical Properties

Melting point:

123-126 °C (dec.)(lit.)

Boiling point:

294.6±9.0 °C(Predicted)

Density 

1.064±0.06 g/cm3(Predicted)

storage temp. 

Keep in dark place,Sealed in dry,Room Temperature

form 

Powder or Crystalline Powder

pka

8.73±0.43(Predicted)

color 

White

Water Solubility 

Insoluble in water.

BRN 

1794023

Safety Information

Hazard Codes 

Xi

Risk Statements 

36/37/38

Safety Statements 

26-36

WGK Germany 

3

HS Code 

29280000

MSDS

• Language:English Provider:SigmaAldrich
• Language:English Provider:ALFA

DI-TERT-BUTYL HYDRAZODICARBOXYLATE Usage And Synthesis

Chemical Properties

White powder

Uses

Di-tert-butyl hydrazodicarboxylate, is used as starting reagent during the four-step synthesis of the aminobicyclopyrazolone hydrochloride. It was used as reagent during Pd-catalyzed amination reactions of halo-pyridine substrates.

Uses

Di-tert-butyl hydrazodiformate was used as starting reagent during the four-step synthesis of the aminobicyclopyrazolone hydrochloride. It was used as reagent during Pd-catalyzed amination reactions of halo-pyridine substrates.

Synthesis Reference(s)

Journal of the American Chemical Society, 82, p. 2725, 1960 DOI: 10.1021/ja01496a018

General Description

Di-tert-butyl hydrazodiformate acts as hydrazine substrate during the preparation of protected pyridylhydrazine derivatives.

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