CYCLODODECYLAMINE
CYCLODODECYLAMINE Basic information
- Product Name:
- CYCLODODECYLAMINE
- Synonyms:
-
- Cyclododecanamine
- TIMTEC-BB SBB003726
- CYCLODODECYLAMINE
- AMINOCYCLODODECANE
- 1-Cyclododecanamine
- Cyclododecylamine,98%
- Cyclododecylamine >
- CAS:
- 1502-03-0
- MF:
- C12H25N
- MW:
- 183.33
- EINECS:
- 216-118-2
- Mol File:
- 1502-03-0.mol
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CYCLODODECYLAMINE Chemical Properties
- Melting point:
- 27-29 °C(lit.)
- Boiling point:
- 122-124 °C7 mm Hg(lit.)
- Density
- 0.9093 (rough estimate)
- refractive index
- 1.487-1.489
- Flash point:
- 250 °F
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 10.98±0.20(Predicted)
- CAS DataBase Reference
- 1502-03-0(CAS DataBase Reference)
- EPA Substance Registry System
- Cyclododecanamine (1502-03-0)
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MSDS
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
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CYCLODODECYLAMINE Usage And Synthesis
Chemical Properties
CLEAR SLIGHTLY YELLOW LIQUID AFTER MELTING
Production Methods
Cyclododecylamine is produced by reduction of cyclododecanone oxime with sodium and an alcohol, by catalytic reduction of nitrocyclododecane with hydrogen, by Ritter reaction of cyclododecene with hydrocyanic acid, or by hydrogenation of cyclododecanone under amination conditions. The reaction of cyclododecylamine with propylene oxide leads to a product that can undergo cyclization to give the fungicide Dodemorph (BASF). The compound behaves chemically as a primary amine.
Purification Methods
It can be purified via the hydrochloride salt m 274-275o (from EtOH) or the picrate m 232-234o, and the free base is distilled preferably at water-pump vacuum [Prelog et al. Helv Chim Acta 33 365 1950].
CYCLODODECYLAMINESupplier
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