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ChemicalBook >  Product Catalog >  Organic Chemistry >  Organic fluorine compound >  Fluorobenzaldehyde series >  2,4,6-Trifluorobenzaldehyde

2,4,6-Trifluorobenzaldehyde

Basic information Uses Safety Supplier Related

2,4,6-Trifluorobenzaldehyde Basic information

Product Name:
2,4,6-Trifluorobenzaldehyde
Synonyms:
  • 2,4,6-TRIFLUOROBENZALDEHYDE
  • 2,4,6-Trilfuorobenzaldehyde
  • 2,4,6-Trifluorobenzaldehyde 98%
  • 2,4,6-Trifluorobenzaldehyde98%
  • 2,4,6-Trifluorobenzaldehyde,97%
  • 2,4,6-Trifluorobenzaldehyde AldrichCPR
  • Benzaldehyde, 2,4,6-trifluoro-
  • 2,4,6-Trifluorobenzaldehyde ISO 9001:2015 REACH
CAS:
58551-83-0
MF:
C7H3F3O
MW:
160.09
Product Categories:
  • Aromatic Aldehydes & Derivatives (substituted)
  • Benzaldehyde
  • Miscellaneous
Mol File:
58551-83-0.mol
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2,4,6-Trifluorobenzaldehyde Chemical Properties

Melting point:
60 °C
Boiling point:
165℃
Density 
1.407
storage temp. 
Inert atmosphere,2-8°C
solubility 
soluble in Methanol
form 
Powder
color 
White to slightly grey
Sensitive 
Air Sensitive
BRN 
6800184
CAS DataBase Reference
58551-83-0(CAS DataBase Reference)
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Safety Information

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-22
Safety Statements 
26-36-37/39
Hazard Note 
Irritant
HS Code 
29130000

MSDS

  • Language:English Provider:ALFA
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2,4,6-Trifluorobenzaldehyde Usage And Synthesis

Uses

2,4,6-Trifluorobenzaldehyde is a type of fluorobenzaldehyde. It is an important organic chemical raw material and intermediate, and can be widely used in the synthesis of pesticides, pharmaceuticals, dyes and resins.

Chemical Properties

White flakes

Synthesis

2000ml four mouth -bottle into tetrahydrofuran 500g, 1,3,5-trifluorobenzene 132g, cooled to -60 ° C, in -60 ~ -90°C,, dropwise; 2. 5N 500ml Butyl lithium, drop about I.5h, add heat insulation 2h, system drops add 80g N, N-dimethylformamide, and 100 g of a tetrahydrofuran solution, control temperature below -60 °C, Then add heat insulation 3h, and heating insulation, heating up to -30 °C, and set aside. Another 3000ml four-mouth bottle into 650g water, 226g 30 % hydrochloric acid, 190g sodium chloride, stirring, then add dropwise at 20 ° C above-mentioned -temperature reaction solution adding completed, insulation 0 5h, layered, Water layer with 200g methyl tert butyl ether extraction Combined organic layer, steaming solvent 2,4,6-Trifluorobenzaldehyde 145 g.

References

[1] Patent: CN104610068, 2016, B. Location in patent: Paragraph 0030; 0031

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