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2,4,6-Trifluorobenzaldehyde

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2,4,6-Trifluorobenzaldehyde Basic information

Product Name:
2,4,6-Trifluorobenzaldehyde
Synonyms:
  • 2,4,6-TRIFLUOROBENZALDEHYDE
  • 2,4,6-Trilfuorobenzaldehyde
  • 2,4,6-Trifluorobenzaldehyde 98%
  • 2,4,6-Trifluorobenzaldehyde98%
  • 2,4,6-Trifluorobenzaldehyde,97%
  • 2,4,6-Trifluorobenzaldehyde AldrichCPR
  • Benzaldehyde, 2,4,6-trifluoro-
  • 2,4,6-Trifluorobenzaldehyde ISO 9001:2015 REACH
CAS:
58551-83-0
MF:
C7H3F3O
MW:
160.09
Product Categories:
  • Aromatic Aldehydes & Derivatives (substituted)
  • Benzaldehyde
  • Miscellaneous
Mol File:
58551-83-0.mol
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2,4,6-Trifluorobenzaldehyde Chemical Properties

Melting point:
60 °C
Boiling point:
165℃
Density 
1.407
storage temp. 
Inert atmosphere,2-8°C
solubility 
soluble in Methanol
form 
Powder
color 
White to slightly grey
Sensitive 
Air Sensitive
BRN 
6800184
CAS DataBase Reference
58551-83-0(CAS DataBase Reference)
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Safety Information

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-22
Safety Statements 
26-36-37/39
Hazard Note 
Irritant
HS Code 
29130000

MSDS

  • Language:English Provider:ALFA
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2,4,6-Trifluorobenzaldehyde Usage And Synthesis

Chemical Properties

White flakes

Synthesis

2000ml four mouth -bottle into tetrahydrofuran 500g, 1,3,5-trifluorobenzene 132g, cooled to -60 ° C, in -60 ~ -90°C,, dropwise; 2. 5N 500ml Butyl lithium, drop about I.5h, add heat insulation 2h, system drops add 80g N, N-dimethylformamide, and 100 g of a tetrahydrofuran solution, control temperature below -60 °C, Then add heat insulation 3h, and heating insulation, heating up to -30 °C, and set aside. Another 3000ml four-mouth bottle into 650g water, 226g 30 % hydrochloric acid, 190g sodium chloride, stirring, then add dropwise at 20 ° C above-mentioned -temperature reaction solution adding completed, insulation 0 5h, layered, Water layer with 200g methyl tert butyl ether extraction Combined organic layer, steaming solvent 2,4,6-Trifluorobenzaldehyde 145 g.

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