Basic information Safety Supplier Related

2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene

Basic information Safety Supplier Related

2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Basic information

Product Name:
2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene
Synonyms:
  • 3,4-DICHLORO-5-NITRO-2-METHYLBENZOTRIFLUORIDE
  • 2,3-DICHLORO-6-TRIFLUOROMETHYL-4-NITROTOLUENE
  • BENZENE, 2,3-DICHLORO-4-METHYL-1-NITRO-5-(TRIFLUOROMETHYL)
  • 2,3-DICHLORO-6-TRIFLUOROMETHYL-4-NITROTOLUENE,99+%
  • 3,4-Dichloro-2-methyl-5-nitrobenzotrifluoride
  • 2,3-Dichloro-4-Methyl-1-nitro-5-(trifluoroMethyl)benzene
CAS:
115571-68-1
MF:
C8H4Cl2F3NO2
MW:
274.02
Mol File:
115571-68-1.mol
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2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Chemical Properties

Boiling point:
270.2±35.0 °C(Predicted)
Density 
1.566±0.06 g/cm3(Predicted)
CAS DataBase Reference
115571-68-1(CAS DataBase Reference)
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Safety Information

HS Code 
2904990090
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2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Usage And Synthesis

Synthesis

Fuming concentrated nitric acid was slowly added dropwise to a solution consisting of 2,3-dichloro-6-trifluoromethyltoluene and concentrated sulfuric acid, with strong stirring, and the reaction temperature was kept at no more than 0??C with an ice-salt thermostatic water bath, and the reaction solution became thicker and thicker during the dropwise process, and solids were precipitated. After the dropwise addition was completed, the solution was stirred at 0 ??C for 3.5 h. At the later stage, the solution became thinner and the color gradually changed to orange. Then the solution was slowly poured into crushed ice with strong stirring, and the white crystals were filtered out immediately after the ice melted, washed with ice water until the effluent was neutral, then drenched with a small amount of ice methanol, and dried under vacuum at 60 ?? to a constant weight, to obtain the target compound 2,3-dichloro-6-(trifluoromethyl)toluene.

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