2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene
2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Basic information
- Product Name:
- 2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene
- Synonyms:
-
- 3,4-DICHLORO-5-NITRO-2-METHYLBENZOTRIFLUORIDE
- 2,3-DICHLORO-6-TRIFLUOROMETHYL-4-NITROTOLUENE
- BENZENE, 2,3-DICHLORO-4-METHYL-1-NITRO-5-(TRIFLUOROMETHYL)
- 2,3-DICHLORO-6-TRIFLUOROMETHYL-4-NITROTOLUENE,99+%
- 3,4-Dichloro-2-methyl-5-nitrobenzotrifluoride
- 2,3-Dichloro-4-Methyl-1-nitro-5-(trifluoroMethyl)benzene
- CAS:
- 115571-68-1
- MF:
- C8H4Cl2F3NO2
- MW:
- 274.02
- Mol File:
- 115571-68-1.mol
2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Chemical Properties
- Boiling point:
- 270.2±35.0 °C(Predicted)
- Density
- 1.566±0.06 g/cm3(Predicted)
- CAS DataBase Reference
- 115571-68-1(CAS DataBase Reference)
2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene Usage And Synthesis
Synthesis
Fuming concentrated nitric acid was slowly added dropwise to a solution consisting of 2,3-dichloro-6-trifluoromethyltoluene and concentrated sulfuric acid, with strong stirring, and the reaction temperature was kept at no more than 0??C with an ice-salt thermostatic water bath, and the reaction solution became thicker and thicker during the dropwise process, and solids were precipitated. After the dropwise addition was completed, the solution was stirred at 0 ??C for 3.5 h. At the later stage, the solution became thinner and the color gradually changed to orange. Then the solution was slowly poured into crushed ice with strong stirring, and the white crystals were filtered out immediately after the ice melted, washed with ice water until the effluent was neutral, then drenched with a small amount of ice methanol, and dried under vacuum at 60 ?? to a constant weight, to obtain the target compound 2,3-dichloro-6-(trifluoromethyl)toluene.
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2,3-Dichloro-6-trifluoromethyl-4-nitrotoluene(115571-68-1)Related Product Information
- 4-Nitrotoluene
- 2-Nitrotoluene
- 3-Nitrotoluene
- DINITROTOLUENE
- Dichloroacetic acid
- 4-Nitrotoluene-2-sulfonic Acid
- 2-Methylbenzotrifluoride
- 2,4,6-Trinitrotoluene
- NITROGEN DIOXIDE
- 3-AMINO-5-CHLOROBENZOTRIFLUORIDE
- 4-Chloro-3-nitrobenzotrifluoride
- 2-METHYL-5-NITROBENZOTRIFLUORIDE
- 3,4-Dichlorobenzotrifluoride
- 3-Chloro-5-nitrobenzotrifluoride
- 2,3-Dichloro-6-(trifluoromethyl)toluene
- 4-CHLORO-2-METHYL-3-NITROBENZOTRIFLUORIDE
- 3-Chloro-4-nitrotoluene
- 3,4-Dichloro-2-nitro-6-(trifluoromethyl)toluene