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3-Prop-2-ynoxypropane-1,2-diol

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3-Prop-2-ynoxypropane-1,2-diol Basic information

Product Name:
3-Prop-2-ynoxypropane-1,2-diol
Synonyms:
  • 3-(2-propynyloxy)propane-1,2-diol
  • 3-Prop-2-ynoxypropane-1,2-diol
  • 1-Propargyl glycerol ether
  • POPDH
  • Propargyl-oxo-propane-2,3-dihydroxy:POPDH
  • Propargyl-oxo-propane-2,3-dihydroxy
  • 3-(2-Propynyloxy)-1,2-propanediol
  • Einecs 237-012-2
CAS:
13580-38-6
MF:
C6H10O3
MW:
130.14
EINECS:
237-012-2
Mol File:
13580-38-6.mol
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3-Prop-2-ynoxypropane-1,2-diol Chemical Properties

Boiling point:
30 °C(Press: 1 Torr)
Density 
1.1341 g/cm3
storage temp. 
2-8°C
pka
13.48±0.20(Predicted)
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3-Prop-2-ynoxypropane-1,2-diol Usage And Synthesis

Uses

3-Prop-2-ynoxypropane-1,2-diol is an electroplating intermediate that can be used to formulate electroplating brighteners, and is used in combination with alkynyl alcohol derivatives to synergise light production and enhance ionic co-deposition.

Synthesis

3-Prop-2-ynoxypropane-1,2-diol is prepared by the reaction of propargyl bromide and (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol. The specific synthesis steps are as follows:
Step 1: propargyl bromide; (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol With sodium hydride In tetrahydrofuran Reflux;
Step 2: With hydrogenchloride In tetrahydrofuran; methanol; water at 20℃; for 8h.

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