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TRIPHENYLPHOSPHINE RESIN

Basic information Safety Supplier Related

TRIPHENYLPHOSPHINE RESIN Basic information

Product Name:
TRIPHENYLPHOSPHINE RESIN
Synonyms:
  • TRIPHENYLPHOSPHINE POL. BOUND, 100-200 M ESH, ~1.6 MMOL/G
  • TRIPHENYLPHOSPHINE POL. BOUND, 200-400 M ESH, ~3 MMOL/G
  • TriphenylphosphineResin1%DvbMesh,1-1.5Mmol/G
  • Triphenylphosphine resin, Crosslinked with 1% DVB, 1.2-1.5 mmol/g, 100-200 mesh
  • Triphenylphosphine resin, 1% crosslinked with DVB
  • 4-DIPHENYLPHOSPHINO POLYSTYRENE RESIN
  • COPOLYMER OF STYRENE AND DIVINYLBENZENE, DIPHENYLPHOSPHINATED
  • DIPHENYLPHOSPHINOBENZOYL NOVAGEL(TM) AM RESIN
CAS:
39319-11-4
MF:
C18H15P
MW:
262.285461
Product Categories:
  • Combinatorial Chemistry
  • Mitsunobu Reaction
  • Phosphines (Mitsunobu Reaction)
  • Polymer-Supported Reagents
  • Resins
  • Synthetic Organic Chemistry
  • Ligand
Mol File:
39319-11-4.mol
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TRIPHENYLPHOSPHINE RESIN Chemical Properties

storage temp. 
2-8°C
form 
Beads
color 
White to yellow
Sensitive 
Air Sensitive
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Safety Information

Hazard Codes 
Xn,Xi
Risk Statements 
22-43-20/21/22-36/37/38
Safety Statements 
36/37-36-26
WGK Germany 
3
10-23
HS Code 
29310099

MSDS

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TRIPHENYLPHOSPHINE RESIN Usage And Synthesis

Chemical Properties

white to yellow beads

Uses

Polymer-bound triphenylphosphine is a solid-supported reagent that can be used as a better alternative to triphenylphosphine in the Mitsunobu reaction.
It can also be used:

  • For the esterification of alkylphosphonic acids using primary alcohols in the presence of iodine and imidazole.
  • To catalyze the conversion of 3-[3-(1,3-dioxolan-2-yl)-1-hydroxypropyl]pyridine to 3-[1-bromo-3-(1,3-dioxolan-2-yl)propyl]pyridine using carbon tetrabromide.
  • To isomerize (Z)-nitro olefins to the (E)-isomers.
  • To prepare polymer-bound ylides which are useful in Wittig reactions.
  • To convert alcohols or carboxylic acids to the corresponding chlorides.
  • In combination with carbon tetrachloride for the coupling N-alkoxycarbonyl α-amino acids and primary amines to form the corresponding amides.

Uses

Triphenylphosphine resin is used for the preparation of polymer bound ylids which are useful for Wittig reactions.

TRIPHENYLPHOSPHINE RESINSupplier

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