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Tert-Butyl 4-Vinylphenyl Carbonate

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Tert-Butyl 4-Vinylphenyl Carbonate Basic information

Product Name:
Tert-Butyl 4-Vinylphenyl Carbonate
Synonyms:
  • 1,1-dimethylethyl4-ethenylphenylcarbonate
  • 4-boc-styrene
  • c-1566
  • carbonicacid,1,1-dimethylethyl4-ethenylphenylester
  • p-tert-butoxycarbonyloxystyrenemonomer
  • 4-(tert-Butoxycarbonyloxy)styrene
  • 4-(TERT-BUTOXYCARBONYLOXY)STYRENE;TERT-BUTYL P-VINYLPHENYL CARBONATE
  • tert-Butyl p-vinylphenyl carbonate
CAS:
87188-51-0
MF:
C13H16O3
MW:
220.26
Mol File:
87188-51-0.mol
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Tert-Butyl 4-Vinylphenyl Carbonate Chemical Properties

Melting point:
27-29 °C(lit.)
Boiling point:
187 °C(lit.)
Density 
1.1101 (rough estimate)
refractive index 
1.5090 (estimate)
Flash point:
>230 °F
InChI
InChI=1S/C13H16O3/c1-5-10-6-8-11(9-7-10)15-12(14)16-13(2,3)4/h5-9H,1H2,2-4H3
InChIKey
GJWMYLFHBXEWNZ-UHFFFAOYSA-N
SMILES
C(OC1=CC=C(C=C)C=C1)(=O)OC(C)(C)C
EPA Substance Registry System
Carbonic acid, 1,1-dimethylethyl 4-ethenylphenyl ester (87188-51-0)
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Safety Information

WGK Germany 
2
RTECS 
FG0460000

MSDS

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Tert-Butyl 4-Vinylphenyl Carbonate Usage And Synthesis

Uses

Used as an intermediate in organic synthesis.

Application

Tert-Butyl 4-Vinylphenyl Carbonate (tBVPC) could be used to synthesize a terpolymer, which is a novel chemically amplified positive photoresist with methyl methacrylate (MMA)triphenylsulfonium salt methacrylate (TPSMA). In addition, Lithographic performance of a PAG-bound polymer resist based on tert-butyl 4-vinyl phenyl carbonate, n-[p-(t-butyloxycarbonyloxy) phenyl]maleimide terpolymers as a novel chemically amplified resist exhibited a positive working behavior. They showed 0.18 μm line pattern at electron beam lithography to indicate that the polymer bounded PAG resists have a potential to fabricate nanostructures[1].

Hazard

Moderately toxic by skin contact. A mild skin irritant.

Synthesis

Tert-Butyl 4-Vinylphenyl Carbonate was prepared by reacting 4-Hydroxystyrene with Di-tert-butyl dicarbonate in prestence of Tetramethylammonium hydroxide in water.

References

[1] Jae Beom Yoo . “Triphenylsulfonium salt methacrylate bound polymer resist for electron beam lithography.” Polymer 55 16 (2014): Pages 3599-3604.

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