4-Chloro-2,6-diMethylbroMo benzene Chemical Properties

Melting point:

22-23℃

Boiling point:

243.5℃

Density 

1.462

Flash point:

119.9℃

storage temp. 

Sealed in dry,Room Temperature

form 

liquid

color 

Clear, light lime/lemon

InChI

InChI=1S/C8H8BrCl/c1-5-3-7(10)4-6(2)8(5)9/h3-4H,1-2H3

InChIKey

CFMPIQSLDJXNPD-UHFFFAOYSA-N

SMILES

C1(C)=CC(Cl)=CC(C)=C1Br

Safety Information

HS Code 

2903998090

4-Chloro-2,6-diMethylbroMo benzene Usage And Synthesis

Synthesis Reference(s)

Synthesis, p. 647, 1985 DOI: 10.1055/s-1985-31292

Synthesis

General procedure for the synthesis of 4-chloro-2,6-dimethylbromobenzene from 4-chloro-2,6-dimethylaniline: the procedure was carried out according to Example 1, with the difference that only 6.95 g (0.025 mol) of FeSO4-7H2O was used.At the end of the reaction 20.7 g of oily product was obtained. The content of 4-chloro-2,6-dimethylbromobenzene in the product was analyzed by gas chromatography (GC) to be 97.1% and the yield was 91% of the theoretical value.

References

[1] Patent: US2010/234652, 2010, A1. Location in patent: Page/Page column 4