ROT 300 Chemical Properties

Density 

1.294±0.06 g/cm3 (20 ºC 760 Torr)

storage temp. 

Refrigerator, under inert atmosphere

solubility 

DMSO (Slightly), Heptane (Very Slightly), Methanol (Slightly)

pka

3.41±0.20(Predicted)

form 

Solid

color 

Dark Red to Very Dark Brown

λmax

577nm(CH2Cl2)(lit.)

InChIKey

ZZSIDSMUTXFKNS-UHFFFAOYSA-N

Safety Information

HS Code 

29339900

ROT 300 Usage And Synthesis

Uses

N,N''-Bis(2,6-diisopropylphenyl)-1,6,7,12-tetraphenoxy-3,4,9,10-perylenetetracarboxylic Diimide has applications in the photosensors and optical detectors.

Synthesis

Synthesis of bis(2,6-diisopropylphenyl)-5,6,12,13-tetraphenoxyanthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H, 9H)-tetraone(PTCDA): PBI-Cl (1.7 g, 2 mmol) was stirred under argon with phenol (1.6 mL, 16 mmol) in N-methyl-pyrrolidone (60 mL) in a 250 mLround flask in the presence of powdered anhydrous K2CO3 (1.1 g,8 mmol). The temperature was maintained at 90 °C overnight under N2. After cooling to room temperature, the reaction liquid was poured into the water and extracted with ethyl acetate. The combined organic layers were dried over anhydrous Na2SO4 and evaporated in a vacuum. The crude product was purified by chromatography (silica gel, ethylacetate: petroleum=1:10). Red solid ROT 300 was obtained. Yield: 92%。

ROT 300(123174-58-3)Related Product Information

• 9,10-Diphenylanthracene