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DL-NORPHENYLEPHRINE HYDROCHLORIDE

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DL-NORPHENYLEPHRINE HYDROCHLORIDE Basic information

Product Name:
DL-NORPHENYLEPHRINE HYDROCHLORIDE
Synonyms:
  • alpha-(aminomethyl)-3-hydroxy-benzenemethanohydrochloride
  • alpha-aminomethyl-3-hydroxy-benzylalcohohydrochloride
  • m-octopaminehydrochloride
  • norfenefrin
  • Phenylephrine Hydrochloride Impurity A
  • α-(AMinoMethyl)-3-hydroxybenzeneMethanol
  • 3-(2-aMino-1-hydroxyethyl)phenol hydrochloride
  • Phenylephrine Impurity A HCl (racemic Norphenylephrine HCl)
CAS:
4779-94-6
MF:
C8H11NO2.ClH
MW:
189.64
EINECS:
225-323-6
Product Categories:
  • Impuritues
  • Amines
  • API
  • Aromatics
  • Intermediates & Fine Chemicals
  • Pharmaceuticals
Mol File:
4779-94-6.mol
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DL-NORPHENYLEPHRINE HYDROCHLORIDE Chemical Properties

Melting point:
162-164 °C(lit.)
storage temp. 
-20°C Freezer, Under Inert Atmosphere
solubility 
DMSO (Slightly), Methanol (Slightly), Water (Slightly)
form 
Solid
color 
White to Off-White
Merck 
14,6699
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Safety Information

Hazard Codes 
Xn
Risk Statements 
22
WGK Germany 
3
RTECS 
DN7400000
HS Code 
2922504500
Toxicity
LD50 oral in rat: 390mg/kg

MSDS

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DL-NORPHENYLEPHRINE HYDROCHLORIDE Usage And Synthesis

Chemical Properties

white to almost white crystalline powder

Originator

Zordel,Grelan,Japan,1970

Uses

rac Norphenylephrine Hydrochloride is an Impurity A of phenylephrine. A phenylephrine derivative as leukotriene D4 antagonists.

Definition

ChEBI: Norfenefrine hydrochloride is a member of phenols.

Manufacturing Process

100 parts of the hydrochloride of meta-hydroxy-ω-aminoacetophenone of melting point 220°C to 222°C (obtainable by brominating metaacetoxyacetophenone, causing the bromoketone to react with sodium iodide, adding hexamethylenetetramine to the iodide in an indifferent solvent and scission of the addition product in acid solution) are shaken in aqueous solution with hydrogen in presence of 2 parts of palladium catalyst until 2 atomic proportions of hydrogen have been absorbed. The catalyst is now filtered and the filtrate evaporated in a vacuum; and the crystalline and completely dry residue is dissolved in absolute alcohol and a precipitate is produced by adding dry ether. The hydrochloride of metahydroxyphenylethanolamine thus obtained forms white crystals of melting point 159°C to 160°C.

Therapeutic Function

Adrenergic

DL-NORPHENYLEPHRINE HYDROCHLORIDESupplier

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