Ethanone, 1-(3-amino-4-methylphenyl)- (9CI)

Product Name: Ethanone, 1-(3-amino-4-methylphenyl)- (9CI)
CAS No.: 17071-24-8
Chemical Name: Ethanone, 1-(3-amino-4-methylphenyl)- (9CI)
Synonyms: 1-(3-amino-4-methyl-phenyl)ethanone;Ethanone, 1-(3-amino-4-methylphenyl)-;1-(3-amino-4-methylphenyl)ethan-1-one;Ethanone, 1-(3-amino-4-methylphenyl)- (9CI);1-(3-amino-4-methylphenyl)ethanone(SALTDATA: FREE)
CBNumber: CB01045633
Molecular Formula: C9H11NO
Formula Weight: 149.19
MOL File: 17071-24-8.mol

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Ethanone, 1-(3-amino-4-methylphenyl)- (9CI) Property

Melting point:: 83 °C
Boiling point:: 306.4±22.0 °C(Predicted)
Density: 1.069±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 3.27±0.10(Predicted)
Appearance: Off-white to yellow Solid
InChI: 1S/C9H11NO/c1-6-3-4-8(7(2)11)5-9(6)10/h3-5H,10H2,1-2H3
InChIKey: MCQYTLIHRDCHHT-UHFFFAOYSA-N
SMILES: O=C(C)C1=CC(N)=C(C)C=C1

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Safety

WGK Germany: WGK 3
HS Code: 2922390090
Storage Class: 11 - Combustible Solids
Hazard Classifications: Acute Tox. 4 Oral

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: A618433
Product name: 1-(3-amino-4-methylphenyl)ethanone
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: A618433
Product name: 1-(3-amino-4-methylphenyl)ethanone
Packaging: 100mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: 8759AA
Product name: 1-(3-Amino-4-methylphenyl)ethanone
Packaging: 1g
Price: $340
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0361228
Product name: 1-(3-AMINO-4-METHYLPHENYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $503.51
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4756-1-1S
Product name: 3'-Amino-4'-methylacetophenone
Packaging: 1g
Price: $516
Updated: 2021/12/16

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Ethanone, 1-(3-amino-4-methylphenyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

5333-27-7

17071-24-8

General procedure for the synthesis of 3-amino-4-methylacetophenone from 3-nitro-4-methylacetophenone: 5% palladium-carbon catalyst (wet state, 100 mg) was added to a solution of ethanol (12 mL) containing 3-nitro-4-methylacetophenone (0.4 g, 2.23 mmol). The reaction flask was evacuated and displaced with hydrogen (repeated three times). After stirring the reaction mixture under hydrogen atmosphere for 3 hours, the catalyst was removed by filtration and the filtrate was concentrated to give 3-amino-4-methylacetophenone (330 mg, 99% yield).

References

[1] Patent: WO2003/90912, 2003, A1. Location in patent: Page/Page column 129
[2] Helvetica Chimica Acta, 2010, vol. 93, # 7, p. 1261 - 1273
[3] ACS Medicinal Chemistry Letters, 2018, vol. 9, # 8, p. 854 - 859
[4] ACS Medicinal Chemistry Letters, 2015, vol. 6, # 7, p. 798 - 803
[5] Patent: CN105481790, 2016, A. Location in patent: Paragraph 0130; 0131; 0132; 0133

Ethanone, 1-(3-amino-4-methylphenyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethanone, 1-(3-amino-4-methylphenyl)- (9CI) Suppliers

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17071-24-8, Ethanone, 1-(3-amino-4-methylphenyl)- (9CI)Related Search:

Ethanone, 1-(3-amino-4-methylphenyl)- (9CI)

1-(3-amino-4-methyl-phenyl)ethanone

1-(3-amino-4-methylphenyl)ethan-1-one

Ethanone, 1-(3-amino-4-methylphenyl)-

1-(3-amino-4-methylphenyl)ethanone(SALTDATA: FREE)

17071-24-8

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