ChemicalBook > CAS DataBase List > 5-Bromo-3-Methoxy-Pyridine2-Carbonitrile

5-Bromo-3-Methoxy-Pyridine2-Carbonitrile

Product Name: 5-Bromo-3-Methoxy-Pyridine2-Carbonitrile
CAS No.: 36057-46-2
Chemical Name: 5-Bromo-3-Methoxy-Pyridine2-Carbonitrile
Synonyms: 5-Bromo-3-methoxypicolinonitrile;5-Bromo-3-Methoxy-Pyridine2-Carbonitrile;5-Bromo-3-methoxy-2-pyridinecarbonitrile;2-Pyridinecarbonitrile, 5-bromo-3-methoxy-
CBNumber: CB01074680
Molecular Formula: C7H5BrN2O
Formula Weight: 213.03
MOL File: 36057-46-2.mol

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5-Bromo-3-Methoxy-Pyridine2-Carbonitrile Property

Boiling point:: 310.9±37.0 °C(Predicted)
Density: 1.65±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: -7.15±0.10(Predicted)
Appearance: White to yellow Solid
InChI: InChI=1S/C7H5BrN2O/c1-11-7-2-5(8)4-10-6(7)3-9/h2,4H,1H3
InChIKey: WIRVBLLSXJUOHZ-UHFFFAOYSA-N
SMILES: C1(C#N)=NC=C(Br)C=C1OC

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Safety

Hazard Codes: T
Risk Statements: 25
Safety Statements: 45
RIDADR: UN 2811 6.1 / PGIII
WGK Germany: 3
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Danger
Hazard statements: H301Toxic if swalloed
Precautionary statements: P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000496
Product name: 5-Bromo-3-methoxypicolinonitrile
Purity: Aldrich
Packaging: 1g
Price: $817
Updated: 2025/07/31

TRC

Product number: B696888
Product name: 5-Bromo-3-methoxy-pyridine2-carbonitrile
Packaging: 250mg
Price: $660
Updated: 2021/12/16

Matrix Scientific

Product number: 035197
Product name: 5-Bromo-3-methoxypicolinonitrile
Packaging: 250mg
Price: $315
Updated: 2021/12/16

AK Scientific

Product number: X2984
Product name: 5-Bromo-3-methoxy-pyridine2-carbonitrile
Packaging: 1g
Price: $583
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0036988
Product name: 5-BROMO-3-METHOXY-PYRIDINE 2-CARBONITRILE
Purity: 95.00%
Packaging: 250MG
Price: $1010.63
Updated: 2021/12/16

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5-Bromo-3-Methoxy-Pyridine2-Carbonitrile Chemical Properties,Usage,Production

Synthesis

886373-28-0

124-41-4

36057-46-2

Sodium methanolate (2.68 g, 49.59 mmol) was added to a solution of 5-bromo-3-fluoropyridine-2-carbonitrile (2.00 g, 9.93 mmol) in tetrahydrofuran (THF, 80 mL) at room temperature. The reaction mixture was stirred at 70 °C for 3 hours. Upon completion of the reaction, the pH of the reaction mixture was adjusted to 7 with a 3 M solution of HCl. The reaction mixture was extracted with ethyl acetate (100 mL x 3). The organic phases were combined, washed with brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give 5-bromo-3-methoxypyridine-2-carbonitrile as a brown solid (2.00 g, 95% yield). Mass spectrum (MS): m/z = 213.0 [M + H]+.

References

[1] Patent: US2016/376283, 2016, A1. Location in patent: Paragraph 1219; 1220
[2] Patent: EP3275864, 2018, A1. Location in patent: Paragraph 0032; 0038; 0044; 0050; 0056; 0062
[3] Patent: WO2007/87488, 2007, A2. Location in patent: Page/Page column 24

5-Bromo-3-Methoxy-Pyridine2-Carbonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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36057-46-2, 5-Bromo-3-Methoxy-Pyridine2-CarbonitrileRelated Search:

Pyridine

5-Bromo-3-Methoxy-Pyridine2-Carbonitrile

5-Bromo-3-methoxypicolinonitrile

2-Pyridinecarbonitrile, 5-bromo-3-methoxy-

5-Bromo-3-methoxy-2-pyridinecarbonitrile

36057-46-2