4,6-Dihydroxy-2-phenylpyrimidine
- Product Name
- 4,6-Dihydroxy-2-phenylpyrimidine
- CAS No.
- 13566-71-7
- Chemical Name
- 4,6-Dihydroxy-2-phenylpyrimidine
- Synonyms
- 2-Phenyl-4,6-pyrimidinediol;6-Hydroxy-2-phenyl-4(1H)-pyrimidinone;4-hydroxy-2-phenyl-1H-pyrimidin-6-one;4(3H)-Pyrimidinone, 6-hydroxy-2-phenyl-
- CBNumber
- CB01106354
- Molecular Formula
- C10H8N2O2
- Formula Weight
- 188.18
- MOL File
- 13566-71-7.mol
4,6-Dihydroxy-2-phenylpyrimidine Property
- Melting point:
- 325-330 °C
- Density
- 1.33±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 5.04±0.10(Predicted)
Safety
- HS Code
- 2933599590
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P399943
- Product name
- 2-Phenyl-pyrimidine-4,6-diol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 5034CB
- Product name
- 2-Phenylpyrimidine-4,6-diol
- Packaging
- 250mg
- Price
- $72
- Updated
- 2021/12/16
- Product number
- 5034CB
- Product name
- 2-Phenylpyrimidine-4,6-diol
- Packaging
- 5g
- Price
- $143
- Updated
- 2021/12/16
- Product number
- CHM0021776
- Product name
- 2-PHENYL-4,6-PYRIMIDINEDIOL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $722.8
- Updated
- 2021/12/16
- Product number
- CHM0021776
- Product name
- 2-PHENYL-4,6-PYRIMIDINEDIOL
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1115.96
- Updated
- 2021/12/16
4,6-Dihydroxy-2-phenylpyrimidine Chemical Properties,Usage,Production
Synthesis
1670-14-0
108-59-8
13566-71-7
Benzamidine hydrochloride (26.0 g, 0.166 mol) and dimethyl malonate (21.9 g, 0.166 mol) were dissolved in anhydrous methanol (200 mL). A methanolic solution of 30% sodium methanol (89.7 g, 0.498 mol) was slowly added under stirring conditions and sodium chloride precipitation was observed to be generated during the reaction. The reaction mixture was stirred continuously at 55°C for 2 hours. After completion of the reaction, the reaction mixture was diluted with water (500 mL) to obtain a clarified solution. Subsequently, it was acidified by dropwise addition of acetic acid (35 mL) and a white precipitate was rapidly precipitated. After continued stirring for 30 min, the solid product was collected by filtration. The filter cake was washed sequentially with water, methanol and acetone and dried to give 2-phenylpyrimidine-4,6-diol in a yield of 25 g (80% yield) as a white solid.
References
[1] Patent: WO2012/167053, 2012, A1. Location in patent: Page/Page column 92
4,6-Dihydroxy-2-phenylpyrimidine Preparation Products And Raw materials
Raw materials
Preparation Products
4,6-Dihydroxy-2-phenylpyrimidine Suppliers
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View Lastest Price from 4,6-Dihydroxy-2-phenylpyrimidine manufacturers
- Product
- 4,6-Dihydroxy-2-phenylpyrimidine 13566-71-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- 100kgs/month
- Release date
- 2021-11-20
- Product
- 4,6-Dihydroxy-2-phenylpyrimidine 13566-71-7
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 500g;1kg; 25kg
- Release date
- 2020-01-10