ChemicalBook > CAS DataBase List > 4-Bromo-5-chloro-2-fluoroaniline

4-Bromo-5-chloro-2-fluoroaniline

Product Name
4-Bromo-5-chloro-2-fluoroaniline
CAS No.
116369-24-5
Chemical Name
4-Bromo-5-chloro-2-fluoroaniline
Synonyms
4-Bromo-5-chloro-2-fluoroaniline;2-Fluoro-4-Bromo-5-Chloroaniline;Benzenamine, 4-bromo-5-chloro-2-fluoro-
CBNumber
CB01115547
Molecular Formula
C6H4BrClFN
Formula Weight
224.46
MOL File
Mol file
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4-Bromo-5-chloro-2-fluoroaniline Property

Boiling point:
258.9±35.0 °C(Predicted)
Density 
1.809±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
1.44±0.10(Predicted)
Appearance
Off-white to gray Solid
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Safety

HS Code 
2921490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B687743
Product name
4-Bromo-5-chloro-2-fluoroaniline
Packaging
100mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
1542CV
Product name
4-Bromo-5-chloro-2-fluoroaniline
Packaging
250mg
Price
$88
Updated
2021/12/16
Apolloscientific
Product number
PC502456
Product name
4-Bromo-5-chloro-2-fluoroaniline
Packaging
1g
Price
$131
Updated
2021/12/16
SynQuest Laboratories
Product number
3630-F-0A
Product name
4-Bromo-5-chloro-2-fluoroaniline
Packaging
1g
Price
$144
Updated
2021/12/16
Apolloscientific
Product number
PC502456
Product name
4-Bromo-5-chloro-2-fluoroaniline
Packaging
5g
Price
$399
Updated
2021/12/16
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4-Bromo-5-chloro-2-fluoroaniline Chemical Properties,Usage,Production

Synthesis

2106-05-0

116369-24-5

General procedure for the synthesis of 4-bromo-5-chloro-2-fluoroaniline from 2-fluoro-5-chloroaniline: N-bromosuccinimide (1 eq.) was added to a solution of 5-chloro-2-fluoroaniline (1 eq.) in acetonitrile (0.5 M) at 25 °C. The reaction mixture was stirred at 25 °C for 1 hour. After completion of the reaction, the mixture was concentrated to dryness and the residue obtained was purified by silica gel column chromatography to afford 4-bromo-5-chloro-2-fluoroaniline in 91% yield as a yellow oil.1H NMR (400 MHz, CDCl3) δppm: 7.23 (d, J = 10.2 Hz, 1H), 6.88 (d, J = 8.4 Hz, 1H), 3.92- 2.64 (br, 2H).

References

[1] Patent: US2016/96841, 2016, A1. Location in patent: Paragraph 0370

4-Bromo-5-chloro-2-fluoroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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116369-24-5, 4-Bromo-5-chloro-2-fluoroanilineRelated Search:

2-fluoro-4-BroMo-5-chlorobenzoic acid 4-CHLORO-2-FLUORO-5-NITROTOLUENE 3-Amino-4-nitrophenol 5-Chloro-2-fluoroaniline

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