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METHOXYACETIC ACID HYDRAZIDE

Product Name
METHOXYACETIC ACID HYDRAZIDE
CAS No.
20605-41-8
Chemical Name
METHOXYACETIC ACID HYDRAZIDE
Synonyms
AKOS B015437;ART-CHEM-BB B015437;METHOXYACETOHYDRAZIDE;2-METHOXYACETOHYDRAZIDE;2-methoxyethanehydrazide;METHOXYACETIC ACID HYDRAZIDE;Acetic acid, 2-methoxy-, hydrazide
CBNumber
CB0119676
Molecular Formula
C3H8N2O2
Formula Weight
104.11
MOL File
20605-41-8.mol
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METHOXYACETIC ACID HYDRAZIDE Property

Melting point:
58-59°C
Boiling point:
271.5±23.0 °C(Predicted)
Density 
1.107±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
form 
Solid
pka
12.29±0.18(Predicted)
Appearance
White to off-white Solid
CAS DataBase Reference
20605-41-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
20/21/22-36/37/38
Safety Statements 
26-36/37/39
HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
M261153
Product name
2-Methoxyacetohydrazide
Packaging
500mg
Price
$40
Updated
2021/12/16
TRC
Product number
M261153
Product name
2-Methoxyacetohydrazide
Packaging
1g
Price
$50
Updated
2021/12/16
Ark Pharm
Product number
AK110451
Product name
2-Methoxyacetohydrazide
Purity
95+%
Packaging
10g
Price
$14
Updated
2021/12/16
Matrix Scientific
Product number
029897
Product name
2-Methoxyacetohydrazide
Packaging
5g
Price
$29
Updated
2021/12/16
ChemScene
Product number
CS-W005634
Product name
2-Methoxyacetohydrazide
Purity
98.92%
Packaging
100g
Price
$95
Updated
2021/12/16
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METHOXYACETIC ACID HYDRAZIDE Chemical Properties,Usage,Production

Uses

2-Methoxyacetohydrazide is used in preparation of Benzylaminopyrazolopyrimidinone derivatives and analogs for use as DNA polymerase IIIC inhibitors.

Synthesis

6290-49-9

20605-41-8

Preparative Example 5: Synthesis of 2-methoxyacetohydrazide Hydrazine monohydrate (9.85 mL, 202 mmol) was slowly added to a solution of methyl methoxyacetate (10 mL, 101 mmol) in methanol (50 mL). The reaction mixture was continuously stirred and heated at 70 °C for 18 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure in a rotary evaporator to remove the solvent. Toluene (2 x 50 mL) was added to the residue for azeotropic dehydration to give a white solid product. The solid was ground with ether (50 mL) for further purification, followed by vacuum drying at 50 °C for 30 min to give the final methoxyacetylhydrazine as a white solid in 95% yield (9.98 g). The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 3.26 (s, 3H), 3.79 (s, 2H), 4.22 (bs, 2H), 8.97 (bs, 1H).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 2, p. 516 - 520
[2] Patent: US2006/160786, 2006, A1. Location in patent: Page/Page column 22
[3] Patent: WO2005/74904, 2005, A2. Location in patent: Page/Page column 57-58
[4] Patent: WO2004/108661, 2004, A1. Location in patent: Page/Page column 51
[5] Patent: WO2005/63742, 2005, A2. Location in patent: Page/Page column 23

METHOXYACETIC ACID HYDRAZIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from METHOXYACETIC ACID HYDRAZIDE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
METHOXYACETIC ACID HYDRAZIDE 20605-41-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-10
Career Henan Chemical Co
Product
METHOXYACETIC ACID HYDRAZIDE 20605-41-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2019-07-03

20605-41-8, METHOXYACETIC ACID HYDRAZIDERelated Search:

Methoxyacetyl chloride 2,4-DICHLOROPHENOXYACETIC ACID HYDRAZIDE 2-CHLOROPHENOXYACETIC ACID HYDRAZIDE 2-(4-CHLORO-2-METHYLPHENOXY)ACETIC ACID HYDRAZIDE Methoxyacetic acid Acethydrazide Hydrazine acetate 4-NITROPHENOXYACETIC ACID HYDRAZIDE 4-FLUOROPHENOXYACETIC ACID HYDRAZIDE 2-METHYL-2-[4-(TRIFLUOROMETHOXY)PHENOXY]ACETIC ACID HYDRAZIDE 4-(TRIFLUOROMETHOXY)PHENOXYACETIC ACID HYDRAZIDE 2-(2-[[(4-CHLOROPHENYL)THIO]METHYL]PHENOXY)ETHANOHYDRAZIDE (2,4-DIBROMO-PHENOXY)-ACETIC ACID HYDRAZIDE N'1-(2-THIENYLMETHYLIDENE)-2-(2-[(4,5-DICHLORO-1H-IMIDAZOL-1-YL)METHYL]PHENOXY)ETHANOHYDRAZIDE 3-(2-(4-FLUOROPHENOXY)ACETYLHYDRAZIDYL)-2-OXOINDOLINE 2-(2,6-DICHLOROPHENYL)-7-METHYL-5-PHENYL-1-OXA-5,6-DIAZASPIRO[2.4]HEPT-6-EN-4-ONE 2-[2-[(4,5-DICHLORO-1H-IMIDAZOL-1-YL)METHYL]PHENOXY]ETHANOHYDRAZIDE N'1-[3-(TRIFLUOROMETHYL)BENZOYL]-2-(2-[(4,5-DICHLORO-1H-IMIDAZOL-1-YL)METHYL]PHENOXY)ETHANOHYDRAZIDE

  • METHOXYACETIC ACID HYDRAZIDE
  • METHOXYACETOHYDRAZIDE
  • ART-CHEM-BB B015437
  • AKOS B015437
  • 2-METHOXYACETOHYDRAZIDE
  • 2-methoxyethanehydrazide
  • Acetic acid, 2-methoxy-, hydrazide
  • 20605-41-8