1-Azetidinesulfonamide(9CI)
- Product Name
- 1-Azetidinesulfonamide(9CI)
- CAS No.
- 654073-32-2
- Chemical Name
- 1-Azetidinesulfonamide(9CI)
- Synonyms
- 102882;CPD1543-A9;1-Azetidinesulfonamide;azetidine-1-sulfonaMide;azetidine-1-sulphonamide;1-Azetidinesulfonamide(9CI);azetidine-1-sulfonamide - [A87170]
- CBNumber
- CB01282980
- Molecular Formula
- C3H8N2O2S
- Formula Weight
- 136.17
- MOL File
- 654073-32-2.mol
1-Azetidinesulfonamide(9CI) Property
- Boiling point:
- 276.3±23.0 °C(Predicted)
- Density
- 1.51±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Store in freezer, under -20°C
- pka
- 11.52±0.20(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C3H8N2O2S/c4-8(6,7)5-2-1-3-5/h1-3H2,(H2,4,6,7)
- InChIKey
- STIUWSWFXIBBKI-UHFFFAOYSA-N
- SMILES
- N1(S(N)(=O)=O)CCC1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- 8971BB
- Product name
- Azetidine-1-sulfonamide
- Packaging
- 100mg
- Price
- $311
- Updated
- 2021/12/16
- Product number
- 120768
- Product name
- Azetidine-1-sulfonamide
- Purity
- 95%
- Packaging
- 1g
- Price
- $1040
- Updated
- 2021/12/16
- Product number
- 101442
- Product name
- 1-Azetidinesulfonamide
- Packaging
- 5g
- Price
- $1600
- Updated
- 2021/12/16
- Product number
- 120768
- Product name
- Azetidine-1-sulfonamide
- Purity
- 95%
- Packaging
- 10g
- Price
- $3200
- Updated
- 2021/12/16
- Product number
- A151397
- Product name
- Azetidine-1-sulfonamide
- Purity
- 95%
- Packaging
- 250mg
- Price
- $190
- Updated
- 2021/12/16
1-Azetidinesulfonamide(9CI) Chemical Properties,Usage,Production
Synthesis
1271835-78-9
654073-32-2
The general procedure for the synthesis of 1-azetidinylsulfonamide using the compound (CAS:1271835-78-9) as starting material was as follows: palladium hydroxide (20%, 350 mg), benzyl (azetidin-1-ylsulfonyl) carbamate (1.49 g, 5.5 mmol), and 1-methyl-1,4-cyclohexadiene (10.7 g, 0.11 mol) of the The mixture was dissolved in methanol (35 mL) and the reaction was stirred at 60 °C under nitrogen protection overnight. After completion of the reaction, the mixture was cooled to room temperature, filtered through a diatomaceous earth pad, and the filtrate was concentrated in vacuum to afford 1-azetidinesulfonamide (437 mg, 58% yield) as a solid product. The product was characterized by 1H NMR (400 MHz, CD3OD) with chemical shifts δ of 2.15 (quintuple peak, 2H) and 3.78 (triplet peak, 4H).The corresponding mass ions were not detected by LCMS analysis.
References
[1] Patent: WO2013/88315, 2013, A1. Location in patent: Page/Page column 75
[2] Patent: WO2013/102826, 2013, A1. Location in patent: Page/Page column 91
1-Azetidinesulfonamide(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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