2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI)
- Product Name
- 2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI)
- CAS No.
- 337904-76-4
- Chemical Name
- 2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI)
- Synonyms
- 6-Isopropylpicolinonitrile;2-Cyano-6-isopropylpyridine;6-Isopropylpyridine-2-carbonitrile;6-(propan-2-yl)pyridine-2-carbonitrile;6-(1-methylethyl)-2-Pyridinecarbonitrile;2-Pyridinecarbonitrile, 6-(1-methylethyl)-;2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI)
- CBNumber
- CB01302253
- Molecular Formula
- C9H10N2
- Formula Weight
- 146.19
- MOL File
- 337904-76-4.mol
2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI) Property
- Boiling point:
- 226.6±28.0 °C(Predicted)
- Density
- 1.02±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 0.29±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C955823
- Product name
- 2-Cyano-6-isopropylpyridine
- Packaging
- 100mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- CS-0050380
- Product name
- 6-Isopropylpyridine-2-carbonitrile
- Packaging
- 100mg
- Price
- $113
- Updated
- 2021/12/16
- Product number
- CS-0050380
- Product name
- 6-Isopropylpyridine-2-carbonitrile
- Packaging
- 250mg
- Price
- $188
- Updated
- 2021/12/16
- Product number
- OR923642
- Product name
- 2-Cyano-6-isopropylpyridine
- Purity
- 95%
- Packaging
- 250mg
- Price
- $225
- Updated
- 2021/12/16
- Product number
- 3H37-1-4W
- Product name
- 6-(Propan-2-yl)pyridine-2-carbonitrile
- Purity
- 97.0%
- Packaging
- 250mg
- Price
- $290
- Updated
- 2021/12/16
2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI) Chemical Properties,Usage,Production
Synthesis
65257-53-6
7677-24-9
337904-76-4
1B: General procedure for the synthesis of 2-cyano-6-isopropylpyridine (105). A mixture of 2-isopropylpyridine-N-oxide (104, 1.33 g, 9.7 mmol) with trimethylcyanosilane (TMS-CN, 1.42 mL, 1.06 g, 11.0 mmol) in 1,2-dichloroethane (40 mL) was stirred at room temperature for 5 min. Subsequently, diethylcarbamoyl chloride (Et2NCOCl, 1.23 mL, 9.7 mmol) was added and stirring was continued at room temperature under inert atmosphere. After 2 days of reaction, 10% aqueous potassium carbonate solution was added and stirring was continued for 10 min. The organic layer was separated and the aqueous layer was extracted twice with 1,2-dichloroethane. The organic layers were combined, washed with brine, dried over anhydrous sodium sulfate and concentrated. The residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate, 3:1) to afford 6-isopropylpyridinecarbonitrile 1.06 g (74% yield): m/z = 147 (M + H)+.
References
[1] Patent: WO2007/14926, 2007, A1. Location in patent: Page/Page column 108
[2] European Journal of Inorganic Chemistry, 2006, # 2, p. 366 - 379
[3] Bioorganic and Medicinal Chemistry Letters, 1998, vol. 8, # 5, p. 453 - 458
2-Pyridinecarbonitrile,6-(1-methylethyl)-(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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