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nooglutil

Product Name
nooglutil
CAS No.
112193-35-8
Chemical Name
nooglutil
Synonyms
ONK-10;Nooglutyl;nooglutil;N-(5-hydroxynicotinoyl)-L-glutamic acid;N-[(5-Hydroxypyridin-3-yl)carbonyl]-L-glutamic acid;N-[(5-Hydroxy-3-pyridinyl)carbonyl]-L-glutamic acid;L-GlutaMic acid, N-[(5-hydroxy-3-pyridinyl)carbonyl]-
CBNumber
CB01328897
Molecular Formula
C11H12N2O6
Formula Weight
268.22
MOL File
112193-35-8.mol
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nooglutil Property

Boiling point:
704.7±60.0 °C(Predicted)
Density 
1.514±0.06 g/cm3(Predicted)
pka
3.15±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
API0025598
Product name
NOOGLUTIL
Purity
95.00%
Packaging
5MG
Price
$501.26
Updated
2021/12/16
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nooglutil Chemical Properties,Usage,Production

Uses

N-(5-hydroxynicotinoyl)-L-glutamic acid can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


A solution of 233 g (5.83 mol) of NaOH in 930 mL of water was added to 345 g of the raw diethyl ester 15 ina 3-L one-neck flask, and the mixture was stirred a troom temperature for 2 h, after which 30 g of activated carbon was added, and stirring was continued for an additional 30 min and filtered on a Buchner funnel tor remove the activated carbon. The filtrate was made acidic (pH 4) by adding 545 mL of conc. HCl and stirred for 1 h. The precipitate was filtered off (Schott filter no. 3), washed with water (3 ?á 600 mL), suspended in 750 mL of water, acidified to pH 4 with 65 mL of conc. HCl, and immediately neutralized to pH 8 with 90 mL of 40% NaOH. Activated carbon, 13 g, was then added, and the mixture was stirred for 30 min, the activated carbon was removed by filtration, and the filtrate was acidified to pH 4 with conc. HCl. The precipitate was filtered off, washed with water (3 ?á 500 mL), and dried at 55 ??C and a vacuum of 40 mmHg for 12 h to obtain 129 g (70%) of the target product, purity by HPLC 99.61%, main substance content by titration 80% (water 21%).

nooglutil Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from nooglutil manufacturers

Hebei Kingfiner Technology Development Co.Ltd
Product
nooglutil 112193-35-8
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
50000kg
Release date
2024-06-03
Hebei Duling International Trade Co. LTD
Product
nooglutil 112193-35-8
Price
US $50.00/kg
Min. Order
1kg
Purity
99%min
Supply Ability
1
Release date
2022-09-26
Nantong Guangyuan Chemicl Co,Ltd
Product
nooglutil 112193-35-8
Price
US $10.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
1000kg
Release date
2023-11-02

112193-35-8, nooglutilRelated Search:


  • nooglutil
  • Nooglutyl
  • N-[(5-Hydroxy-3-pyridinyl)carbonyl]-L-glutamic acid
  • N-[(5-Hydroxypyridin-3-yl)carbonyl]-L-glutamic acid
  • ONK-10
  • L-GlutaMic acid, N-[(5-hydroxy-3-pyridinyl)carbonyl]-
  • N-(5-hydroxynicotinoyl)-L-glutamic acid
  • 112193-35-8