6-BROMO-2-CHLORO-4-METHYLQUINOLINE

Product Name: 6-BROMO-2-CHLORO-4-METHYLQUINOLINE
CAS No.: 3913-19-7
Chemical Name: 6-BROMO-2-CHLORO-4-METHYLQUINOLINE
Synonyms: Lepidine, 6-bromo-2-chloro-;BROMO-2-CHLORO-4-METHYLQUINOLINE;2-Chloro-4-Methyl-6-broMoquinoline;6-BROMO-2-CHLORO-4-METHYLQUINOLINE;Quinoline, 6-bromo-2-chloro-4-methyl-
CBNumber: CB01479904
Molecular Formula: C10H7BrClN
Formula Weight: 256.53
MOL File: 3913-19-7.mol

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6-BROMO-2-CHLORO-4-METHYLQUINOLINE Property

Melting point:: 140 °C
Boiling point:: 347.6±37.0 °C(Predicted)
Density: 1.591±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 0.15±0.50(Predicted)
Appearance: Off-white to light brown Solid

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

H413May cause long lasting harmful effects to aquatic life

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: BBO000343
Product name: 6-Bromo-2-chloro-4-methylquinoline
Purity: Aldrich
Packaging: 1g
Price: $241
Updated: 2023/01/07

TRC

Product number: B690753
Product name: 6-Bromo-2-chloro-4-methylquinoline
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B690753
Product name: 6-Bromo-2-chloro-4-methylquinoline
Packaging: 250mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0107850
Product name: 6-BROMO-2-CHLORO-4-METHYL-QUINOLINE
Purity: 95.00%
Packaging: 250MG
Price: $176.4
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-D-1A
Product name: 6-Bromo-2-chloro-4-methylquinoline
Packaging: 1g
Price: $240
Updated: 2021/12/16

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6-BROMO-2-CHLORO-4-METHYLQUINOLINE Chemical Properties,Usage,Production

Synthesis

89446-19-5

3913-19-7

General procedure for the synthesis of 6-bromo-2-chloro-4-methylquinoline from 6-bromo-4-methyl-2(1H)-quinolinone: 25 mL of phosphorochloridic acid was added to 2.7 g (11.34 mmol) of 6-bromo-4-methyl-1H-quinolin-2-one (Example 1b), and the reaction mixture was refluxed for 2 hours. Upon completion of the reaction, it was cooled to room temperature and the mixture was slowly poured into 250 mL of 10% ammonia solution to precipitate. The precipitate was collected by filtration, washed with water and dried in a circulating air dryer at 30 °C. A product of 2.7 g was obtained in 93% yield. Product characterization: C10H7BrClN (M = 256.526); calculated molecular ion peak (M + H)+: 256/258/260 (BrCl); measured molecular ion peak (M + H)+: 256/258/260 (BrCl); Rf value: 0.95 (silica gel, dichloromethane/methanol 9:1).

References

[1] Journal of Medicinal Chemistry, 1989, vol. 32, # 8, p. 1936 - 1942
[2] Synthesis, 2011, # 6, p. 934 - 942
[3] Patent: US2005/234101, 2005, A1. Location in patent: Page/Page column 14
[4] Patent: WO2005/103002, 2005, A2. Location in patent: Page/Page column 44-45
[5] Patent: US2005/267115, 2005, A1. Location in patent: Page/Page column 33

6-BROMO-2-CHLORO-4-METHYLQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BROMO-2-CHLORO-4-METHYLQUINOLINE Suppliers

China 57 India 1 Japan 1 United Kingdom 1 United States 7 Global 67

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View Lastest Price from 6-BROMO-2-CHLORO-4-METHYLQUINOLINE manufacturers

Career Henan Chemical Co

Product: 6-BROMO-2-CHLORO-4-METHYLQUINOLINE 3913-19-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500KG
Release date: 2018-08-19

3913-19-7, 6-BROMO-2-CHLORO-4-METHYLQUINOLINERelated Search:

6-Bromo-2-methylquinoline 6-broMo-2-chlorothiazolo[5,4-b]pyridine 6-bromo-2-chloropyrido[2,3-d]pyrimidine 6-BroMo-2-chloro-8-fluoroquinazoline 6-Bromo-2-chloronicotinic acid 6-BROMO-2-CHLOROQUINAZOLIN-4-AMINE Methyl 6-bromo-2-chloronicotinate 6-Bromo-2-chloro-5-hydroxypyridine 6-Bromo-2-chloro-3-nitropyridine 6-bromo-2-chloroquinoxaline 6-BROMO-2-CHLORO-[1,8]NAPHTHYRIDINE METHYL 6-BROMO-2-OXO-1,2,3,4-TETRAHYDRO-1,8-NAPHTHYRIDINE-3-CARBOXYLATE 6-Bromo-2-chloronicotinaldehyde 6-BROMO-2-CHLOROQUINOLINE-4-CARBOXYLIC ACID, 97 6-BROMO-2-CHLORO-4-METHYLQUINOLINE METHYL 6-BROMO-2-CHLOROQUINOLINE-4-CARBOXYLATE 6-BROMO-2-CHLOROQUINOLINE-4-CARBONYL CHLORIDE 6-BROMO-2-CHLORO-4-PHENYLQUINOLINE

6-BROMO-2-CHLORO-4-METHYLQUINOLINE

2-Chloro-4-Methyl-6-broMoquinoline

Lepidine, 6-bromo-2-chloro-

Quinoline, 6-bromo-2-chloro-4-methyl-

BROMO-2-CHLORO-4-METHYLQUINOLINE

3913-19-7

3913-19-1

90222-58-4