(5-CHLORO-2-METHOXYPHENYL)ACETONITRILE

Product Name: (5-CHLORO-2-METHOXYPHENYL)ACETONITRILE
CAS No.: 7048-38-6
Chemical Name: (5-CHLORO-2-METHOXYPHENYL)ACETONITRILE
Synonyms: 5-Chloro-2-methoxybenzeneacetonitrile;Benzeneacetonitrile, 5-chloro-2-methoxy-;2-(5-chloro-2-Methoxyphenyl)acetonitrile
CBNumber: CB01489169
Molecular Formula: C9H8ClNO
Formula Weight: 181.62
MOL File: 7048-38-6.mol

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(5-CHLORO-2-METHOXYPHENYL)ACETONITRILE Property

Melting point:: 63 °C(Solv: water (7732-18-5); ethanol (64-17-5))
Boiling point:: 138-140 °C(Press: 1 Torr)
Density: 1.198±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C374538
Product name: (5-chloro-2-methoxyphenyl)acetonitrile
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139752
Product name: (5-Chloro-2-methoxyphenyl)acetonitrile
Packaging: 500mg
Price: $70
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139752
Product name: (5-Chloro-2-methoxyphenyl)acetonitrile
Packaging: 1g
Price: $119
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139752
Product name: (5-Chloro-2-methoxyphenyl)acetonitrile
Packaging: 2g
Price: $207
Updated: 2021/12/16

AK Scientific

Product number: 0911AC
Product name: (5-Chloro-2-methoxyphenyl)acetonitrile
Packaging: 1g
Price: $215
Updated: 2021/12/16

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(5-CHLORO-2-METHOXYPHENYL)ACETONITRILE Chemical Properties,Usage,Production

Synthesis

773837-37-9

7035-11-2

7048-38-6

The general procedure for the synthesis of 5-chloro-2-methoxyphenylacetonitrile from the compound (CAS: 773837-37-9) and 4-chloro-2-(chloromethyl)-1-methoxybenzene was as follows: compound Z-0-6 (32 g, 168 mmol) was dissolved in dimethyl sulfoxide (DMSO, 200 mL). Subsequently, sodium cyanide (29 g, 606 mmol) was added to the solution. The reaction mixture was heated to 80 °C under nitrogen protection and maintained at this temperature for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature, dispersed by the addition of water, and the product was subsequently separated by diafiltration. The filter cake was washed with a small amount of water and dried to give Z-0-7 (31 g, yield: 98.3%) as an orange-red solid.

References

[1] Patent: CN106243003, 2016, A. Location in patent: Paragraph 0130; 0131; 0136
[2] Patent: US2016/130239, 2016, A1. Location in patent: Paragraph 0735; 0739
[3] Patent: WO2014/151472, 2014, A1. Location in patent: Paragraph 00398-00399
[4] Patent: WO2016/40315, 2016, A1. Location in patent: Paragraph 00441; 00442
[5] Journal of Medicinal Chemistry, 2017, vol. 60, # 16, p. 7029 - 7042

(5-CHLORO-2-METHOXYPHENYL)ACETONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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(5-CHLORO-2-METHOXYPHENYL)ACETONITRILE Suppliers

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7048-38-6, (5-CHLORO-2-METHOXYPHENYL)ACETONITRILERelated Search:

Benzeneacetonitrile ACETONE-D6 2-Methoxyphenylacetonitrile

2-(5-chloro-2-Methoxyphenyl)acetonitrile

Benzeneacetonitrile, 5-chloro-2-methoxy-

5-Chloro-2-methoxybenzeneacetonitrile

7048-38-6