ChemicalBook > CAS DataBase List > 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE

1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE

Product Name: 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE
CAS No.: 39930-11-5
Chemical Name: 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE
Synonyms: alpha-(2-Pyridyl)benzylamine;α-Phenyl-2-pyridineMethanaMine;2-PyridineMethanaMine, α-phenyl;(R)-phenyl(pyridin-2-yl)methanamine
CBNumber: CB01489341
Molecular Formula: C12H12N2
Formula Weight: 184.24
MOL File: 39930-11-5.mol

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1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE Property

Melting point:: 54-55 °C
Boiling point:: 159-165 °C(Press: 3 Torr)
Density: 1.106±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 7.51±0.10(Predicted)
Appearance: Light yellow to brown Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 119043
Product name: Phenyl(pyridin-2-yl)methanamine
Purity: 95+%
Packaging: 1g
Price: $226
Updated: 2021/12/16

AK Scientific

Product number: W6032
Product name: Phenyl(pyridin-2-yl)methanamine
Packaging: 5g
Price: $427
Updated: 2021/12/16

Matrix Scientific

Product number: 119043
Product name: Phenyl(pyridin-2-yl)methanamine
Purity: 95+%
Packaging: 5g
Price: $684
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0119239
Product name: 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE
Purity: 95.00%
Packaging: 1G
Price: $808.89
Updated: 2021/12/16

Matrix Scientific

Product number: 119043
Product name: Phenyl(pyridin-2-yl)methanamine
Purity: 95+%
Packaging: 10g
Price: $1080
Updated: 2021/12/16

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1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

1826-28-4

39930-11-5

The general procedure for the synthesis of 3-(2-pyridyl)aniline from phenyl-2-pyridyl ketoxime was as follows: phenyl(2-pyridyl)ketoxime (5.0 g, 25.2 mmol) was dissolved in ice-cold mixed solvent of acetic acid (50 mL) and ethanol (100 mL). Under stirring, zinc powder (50 g) was added in batches of 2 g. After addition, the reaction mixture was stirred at room temperature for 24 hours. After completion of the reaction, the unreacted zinc powder was removed by filtration and washed well with ethanol. The filtrate and washings were combined and concentrated under reduced pressure. Several 10 mL of water were added to the concentrate and the acetic acid was removed by evaporation. The pH of the mixture was adjusted to about 12 with aqueous KOH and then extracted with diethyl ether (3 x 50 mL). The organic phases were combined, dried over anhydrous Na2SO4, and the solvent was evaporated under reduced pressure to afford the target product 3-(2-pyridyl)aniline in a yield of 4.5 g (96.8% yield). The product was subjected to IR, 1H NMR, 13C NMR and elemental analysis to confirm the structure.IR (KBr, cm-1): 3445(b), 3307(b), 3255(s), 3180(s), 3101(w), 1630(s), 1604(s), 1549(w), 1519(s), 1477(s), 1466(s), 1441(s), 1363(s). 1441(s), 1363(s), 1282(s), 1252(s), 1211(w), 1161(w), 1097(s), 1038(s), 766(s), 658(w), 640(w), 543(s).1H NMR (400 MHz, CDCl3): δ 8.53 (1H, d, J=4.8Hz ), 7.56(1H, t, J=7.6Hz), 7.39(1H, d, J=8.0Hz), 7.30(1H, t, J=7.6Hz), 7.24(1H, t, J=6.4Hz), 7.19(1H, d, J=6.4Hz), 7.10(1H, t, J=6.2Hz), 5.21(1H, s), 5.21(1H, s). 2.75 (2H, s, NH2).13C NMR (100 MHz, CDCl3): δ 158.6, 154.2, 149.6, 136.7, 131.0, 129.2, 128.7, 128.5, 123.1, 56.2. Elemental analysis (C12H12N2) calculated values: C, 78.23; H, 6.57; N Calculated values for elemental analysis (C12H12N2): C, 78.23; H, 6.57; N, 15.21. Measured values: C, 77.64; H, 5.98; N, 15.13%.

References

[1] Inorganica Chimica Acta, 2012, vol. 390, p. 154 - 162
[2] Inorganica Chimica Acta, 2013, vol. 394, p. 210 - 219
[3] European Journal of Inorganic Chemistry, 2010, # 12, p. 1791 - 1797
[4] Journal of Organic Chemistry, 2009, vol. 74, # 9, p. 3566 - 3568

1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE manufacturers

Career Henan Chemical Co

Product: 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE 39930-11-5
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

39930-11-5, 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDERelated Search:

Pyridine 4-BENZOYLPIPERIDINE HYDROCHLORIDE Phenyl(2-pyridyl)methylamine hydrochloride 1-PYRIDIN-2-YLETHANAMINE 2-(4-CHLOROPHENYL)-2-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-2-MORPHOLINOACETONITRILE 1-PHENYL-1-PYRIDIN-2-YLMETHANAMINE DIHYDROCHLORIDE

α-Phenyl-2-pyridineMethanaMine

2-PyridineMethanaMine, α-phenyl

(R)-phenyl(pyridin-2-yl)methanamine

alpha-(2-Pyridyl)benzylamine

39930-11-5