ChemicalBook > CAS DataBase List > 2-BROMO-1-ISOPROPYL-4-NITROBENZENE

2-BROMO-1-ISOPROPYL-4-NITROBENZENE

Product Name
2-BROMO-1-ISOPROPYL-4-NITROBENZENE
CAS No.
101980-41-0
Chemical Name
2-BROMO-1-ISOPROPYL-4-NITROBENZENE
Synonyms
1-Bromo-2-isopropyl-5-nitrobenzene;2-Bromo-4-nitro-1-isopropylbenzene;2-BROMO-1-ISOPROPYL-4-NITROBENZENE;2-BROMO-4-NITRO ISO PROPYL BENZENE;2-bromo-4-nitro-1-propan-2-ylbenzene;Benzene, 2-bromo-1-(1-methylethyl)-4-nitro-
CBNumber
CB01511419
Molecular Formula
C9H10BrNO2
Formula Weight
244.09
MOL File
101980-41-0.mol
More
Less

2-BROMO-1-ISOPROPYL-4-NITROBENZENE Property

Boiling point:
155-160 °C(Press: 15 Torr)
Density 
1.456±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
Colorless to light yellow Liquid
More
Less

Hazard and Precautionary Statements (GHS)

More
Less

N-Bromosuccinimide Price

TRC
Product number
B111365
Product name
2-Bromo-1-isopropyl-4-nitrobenzene
Packaging
100mg
Price
$110
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141945
Product name
2-Bromo-1-isopropyl-4-nitrobenzene
Packaging
100mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141945
Product name
2-Bromo-1-isopropyl-4-nitrobenzene
Packaging
250mg
Price
$130
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141945
Product name
2-Bromo-1-isopropyl-4-nitrobenzene
Packaging
500mg
Price
$225
Updated
2021/12/16
AK Scientific
Product number
Z3807
Product name
2-Bromo-1-isopropyl-4-nitrobenzene
Packaging
1g
Price
$237
Updated
2021/12/16
More
Less

2-BROMO-1-ISOPROPYL-4-NITROBENZENE Chemical Properties,Usage,Production

Synthesis

1817-47-6

101980-41-0

General procedure for the synthesis of 2-bromo-1-isopropyl-4-nitrobenzene from 1-isopropyl-4-nitrobenzene: A mixed solution of 1-isopropyl-4-nitrobenzene (50 g, 0.300 mol, GC purity: 99.1%) and ferric chloride (III) was heated to 40 °C and bromine (59.92 g, 0.375 mol) was added slowly and dropwise over a period of 3 hours. After completion of the reaction, the reaction mixture was poured into 120 ml of water and a 40% concentration of aqueous sodium bisulfite (20.81 g, 0.078 mol) was added dropwise. Subsequently, the mixture was extracted with 100 ml of chlorobenzene. After separating the organic phase, the chlorobenzene phase was washed with 100 ml of 5% concentration aqueous HCl solution. Finally, the chlorobenzene was evaporated under reduced pressure to afford 2-bromo-1-isopropyl-4-nitrobenzene (74.05 g, GC purity: 96.9%, yield: 98% of the theoretical value), the product was a yellow oily substance. 1H-NMR (600 MHz, CDCl3) data were as follows: δ= 8.41 (d, 1H), 8.14 (dd, 1H), 7.45 (d, 1H ), 3.45 (heptet, 1H), 1.29 (d, 3H), 1.27 (d, 3H) ppm. GC-MS analysis: m/z = 245 [M+].

References

[1] Patent: WO2013/160387, 2013, A1. Location in patent: Page/Page column 22-23
[2] Patent: WO2009/55674, 2009, A1. Location in patent: Page/Page column 68
[3] Journal of the Chemical Society, 1952, p. 4443,4445
[4] Patent: WO2013/96151, 2013, A1. Location in patent: Page/Page column 93
[5] Patent: EP3312172, 2018, A1. Location in patent: Paragraph 0313; 0314

2-BROMO-1-ISOPROPYL-4-NITROBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

2-BROMO-1-ISOPROPYL-4-NITROBENZENE Suppliers

China 57 India 3 United Kingdom 1 United States 6 Global 67
Shanghai Harvest Chemical Industrial Co., Ltd.
Tel
021-31038972,31038973 17321035817
Fax
+86-21-51385350
Email
sales@harvest-chem.com
Country
China
ProdList
2819
Advantage
64
Wuhan ariel chemical Co., LTD.
Tel
18986259541 18986259541
Fax
027-87840182
Email
sales@3stc.com
Country
China
ProdList
3701
Advantage
58
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66113011 17714375163
Fax
(1)02557626880
Email
cfzhang@aikonchem.com
Country
China
ProdList
19906
Advantage
55
Shanghai Jian Chao Chemical Technology Co., Ltd.
Tel
150-2103-5486 18017383231
Fax
qq：2817624287
Email
983544897@qq.com
Country
China
ProdList
9341
Advantage
55
Bide Pharmatech Ltd.
Tel
400-400-164-7117 18317119277
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39999
Advantage
60
Quzhou Rundong Chemical (Technology) Co.
Tel
0570-8789886 18892685668
Fax
0570-8789985
Email
info@rundongchemical.com
Country
China
ProdList
4053
Advantage
60
Quzhou AMK BioTech Co., Ltd
Tel
0570-3081766 18357083060
Fax
0570-3072337
Email
sales@qzamkbio.com
Country
China
ProdList
1156
Advantage
55
Chengdu Xiaojia Technology Co., Ltd.
Tel
15902830537
Email
zhanghao@happysyn.com
Country
China
ProdList
3123
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Shanghai CR Corporation Limited
Tel
13062833949; 4006653949 4006653949
Fax
QQ: 2136646215
Email
fred.wen@crcorporation.cn
Country
China
ProdList
9730
Advantage
58
More
Less

View Lastest Price from 2-BROMO-1-ISOPROPYL-4-NITROBENZENE manufacturers

Career Henan Chemical Co
Product
2-Bromo-1-isopropyl-4-nitrobenzene 101980-41-0
Price
US $9.80/KG
Min. Order
1KG
Purity
＞98%HPLC
Supply Ability
20 tons
Release date
2020-02-06

101980-41-0, 2-BROMO-1-ISOPROPYL-4-NITROBENZENERelated Search:

1-BROMO-2-CHLORO-3-NITROBENZENE 1-ISOPROPYL-4-NITROBENZENE

  • 2-BROMO-1-ISOPROPYL-4-NITROBENZENE
  • 2-Bromo-4-nitro-1-isopropylbenzene
  • 1-Bromo-2-isopropyl-5-nitrobenzene
  • 2-bromo-4-nitro-1-propan-2-ylbenzene
  • Benzene, 2-bromo-1-(1-methylethyl)-4-nitro-
  • 2-BROMO-4-NITRO ISO PROPYL BENZENE
  • 101980-41-0