4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE
- Product Name
- 4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE
- CAS No.
- 3470-46-0
- Chemical Name
- 4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE
- Synonyms
- 2-Carboxy-5-oxo-5,6,7,8-tetrahydronaphthalene;5-Oxo-7,8-dihydro-6H-naphthalene-2-carboxylic Acid;4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE;4-[(4-METHYLPHENYL)SULPHONYL]PIPERIDINE HYDROCHLORIDE;2-Naphthalenecarboxylic acid, 5,6,7,8-tetrahydro-5-oxo-;5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid 96%;6-Carboxy-1-oxo-1,2,3,4-tetrahydronaphthalene, 5-Oxo-5,6,7,8-tetrahydro-2-naphthoic acid
- CBNumber
- CB0156011
- Molecular Formula
- C11H10O3
- Formula Weight
- 190.2
- MOL File
- 3470-46-0.mol
4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE Property
- Melting point:
- 230(dec.)
- Boiling point:
- 230 °C/dec)
- Density
- 1.309±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 3.77±0.20(Predicted)
- form
- solid
- color
- Light brown
Safety
- Hazard Codes
- Xi,C
- HazardClass
- IRRITANT
- HS Code
- 2902900000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P309+P311IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- O990155
- Product name
- 5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylicAcid
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 012588
- Product name
- 5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid
- Purity
- 98%
- Packaging
- 1g
- Price
- $135
- Updated
- 2021/12/16
- Product number
- 2629-1-X9
- Product name
- 5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid
- Purity
- 96%
- Packaging
- 1g
- Price
- $144
- Updated
- 2021/12/16
- Product number
- 2629-1-X9
- Product name
- 5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid
- Purity
- 96%
- Packaging
- 5G
- Price
- $416
- Updated
- 2021/12/16
- Product number
- 4211AB
- Product name
- 5-Oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylicacid
- Packaging
- 10g
- Price
- $477
- Updated
- 2021/12/16
4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
144464-66-4
3470-46-0
Methyl 5-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate (320 mg, 1.57 mmol) was used as a raw material and dissolved in a solvent mixture of 6 mL of methanol and 3 mL of water. Subsequently, lithium hydroxide (331 mg, 7.88 mmol) was added. The reaction mixture was stirred at room temperature for 1 h. The progress of the reaction was monitored by thin-layer chromatography (TLC), and after confirming that the reaction was complete, the pH of the reaction solution was adjusted to 5 with 1 N hydrochloric acid solution.The reaction solution was concentrated by rotary evaporation and extracted with ethyl acetate (50 mL × 2). The ethyl acetate extracts were combined and the solvent was removed by rotary evaporation to afford the white solid product 5-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid (310 mg, 100% yield).
References
[1] Patent: CN104844471, 2017, B. Location in patent: Paragraph 0186; 0187; 0188
4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE Suppliers
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View Lastest Price from 4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE manufacturers
- Product
- 4-[(4-METHYLPHENYL)SULFONYL]PIPERIDINE HYDROCHLORIDE 3470-46-0
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02