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(R)-1-(2,4-Dichlorophenyl)ethanamine

Product Name
(R)-1-(2,4-Dichlorophenyl)ethanamine
CAS No.
133773-29-2
Chemical Name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Synonyms
EOS-60919;(R)-1-(2,4-chlorophenyl)ethanaMine;(R)-1-(2,4-DICHLOROPHENYL)ETHANAMINE;(1R)-1-(2,4-dichlorophenyl)ethylamine;(R)-1-(2,4-dichlorophenyl)ethan-1-amine;(1R)-1-(2,4-DICHLOROPHENYL)ETHAN-1-AMINE;Benzenemethanamine, 2,4-dichloro-α-methyl-, (αR)-;(1R)-1-(2,4-Dichlorophenyl)ethanamine Hydrochloride
CBNumber
CB0168881
Molecular Formula
C8H9Cl2N
Formula Weight
190.07
MOL File
Mol file
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(R)-1-(2,4-Dichlorophenyl)ethanamine Property

Boiling point:
256.4±25.0 °C(Predicted)
Density 
1.262±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
8.28±0.10(Predicted)
form 
liquid
color 
Colourless
optical activity
37.568°(C=0.01g/ml ETOH)
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Safety

HS Code 
2921490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D475303
Product name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Packaging
2.5mg
Price
$45
Updated
2021/12/16
TRC
Product number
D475303
Product name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Packaging
5mg
Price
$60
Updated
2021/12/16
TRC
Product number
D475303
Product name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Packaging
25mg
Price
$175
Updated
2021/12/16
AK Scientific
Product number
1178AL
Product name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Packaging
1g
Price
$348
Updated
2021/12/16
Apolloscientific
Product number
OR944487
Product name
(R)-1-(2,4-Dichlorophenyl)ethanamine
Purity
95%
Packaging
1g
Price
$646
Updated
2021/12/16
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(R)-1-(2,4-Dichlorophenyl)ethanamine Chemical Properties,Usage,Production

Synthesis

(5)-Mandelic acid (40.2 g, 264.5 mmol) was added to a solution of 3:2 isopropyl alcohol (/PrOH) and ethanol (EtOH) (500 mL) at room temperature, and the suspension was heated at 60 °C until a clear solution formed. Racemic 2,4-dichloro-a-methyl benzylamine (50 g, 264.5 mmol) was added to the hot solution, which was then cooled to 30 °C over 2 h and stirred at this temperature for 24 h. The colorless crystals were collected by filtration and washed with acetone (70 mL). The resulting salt was suspended in 3:2 /PrOH/EtOH (400 mL) at room temperature and the mixture was heated at 60 °C to give a clear solution. The solution was then cooled to room temperature and stirred for 24 hours. The colorless crystals were filtered off, and washed with acetone (40 mL) to give the desired salt. A portion of the salt (12.0 g) in dichloromethane (CH2C12) (100 mL) was added to aqueous 4 N sodium hydroxide solution (30 mL). The reaction mixture was stirred for 1 h at room temperature, and extracted with dichloromethane (2 χ 100 mL), dried with anhydrous sodium sulfate (Na2S04), filtered, and concentrated in vacuo to afford (R)-1-(2,4-Dichlorophenyl)ethanamine as a colorless liquid (7.5 g, 39.5 mmol, 40%).

References

[1] Patent: WO2013/82429, 2013, A1. Location in patent: Paragraph 0115
[2] Patent: WO2013/82490, 2013, A1. Location in patent: Paragraph 0102

(R)-1-(2,4-Dichlorophenyl)ethanamine Preparation Products And Raw materials

Raw materials

Preparation Products

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(R)-1-(2,4-Dichlorophenyl)ethanamine Suppliers

PharmaBlock Sciences (Nanjing),Inc.
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sales@pharmablock.com
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China
ProdList
5000
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55
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China
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+86-21-61629029
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product02@bidepharm.com
Country
China
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Tel
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Fax
Email: sales@rosewellchem.com
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Wuxi Zhongkun Biochemical Technology Co., Ltd.
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Shanghai YuanYe Biotechnology Co., Ltd.
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China
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View Lastest Price from (R)-1-(2,4-Dichlorophenyl)ethanamine manufacturers

Career Henan Chemical Co
Product
(1R)-1-(2,4-Dichlorophenyl)ethanamine 133773-29-2
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2018-12-25

133773-29-2, (R)-1-(2,4-Dichlorophenyl)ethanamineRelated Search:


  • (R)-1-(2,4-DICHLOROPHENYL)ETHANAMINE
  • (1R)-1-(2,4-DICHLOROPHENYL)ETHAN-1-AMINE
  • (R)-1-(2,4-chlorophenyl)ethanaMine
  • (R)-1-(2,4-dichlorophenyl)ethan-1-amine
  • (1R)-1-(2,4-Dichlorophenyl)ethanamine Hydrochloride
  • (1R)-1-(2,4-dichlorophenyl)ethylamine
  • EOS-60919
  • Benzenemethanamine, 2,4-dichloro-α-methyl-, (αR)-
  • 133773-29-2