1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER

Product Name: 1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER
CAS No.: 38588-64-6
Chemical Name: 1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER
Synonyms: 3,5-bis(methoxycarbonyl)benzoicaci;3,5-di(methoxycarbonyl)benzoic acid;3,5-bis(Methoxycarbonyl)benzoic acid;1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER;1,3,5-Benzenetricarboxylic acid, 1,3-dimethyl ester
CBNumber: CB0181080
Molecular Formula: C11H10O6
Formula Weight: 238.19
MOL File: 38588-64-6.mol

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1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER Property

Melting point:: 264 °C (decomp)(Solv: water (7732-18-5))
Boiling point:: 415.1±35.0 °C(Predicted)
Density: 1.340±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 3.46±0.10(Predicted)
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0010337
Product name: 3,5-Bis(methoxycarbonyl)benzoicacid
Purity: 97.60%
Packaging: 100mg
Price: $98
Updated: 2021/12/16

ChemScene

Product number: CS-0010337
Product name: 3,5-Bis(methoxycarbonyl)benzoicacid
Purity: 97.60%
Packaging: 250mg
Price: $157
Updated: 2021/12/16

AK Scientific

Product number: 2300AL
Product name: 3,5-Bis(methoxycarbonyl)benzoicacid
Packaging: 100mg
Price: $174
Updated: 2021/12/16

AK Scientific

Product number: 2300AL
Product name: 3,5-Bis(methoxycarbonyl)benzoicacid
Packaging: 250mg
Price: $247
Updated: 2021/12/16

ChemScene

Product number: CS-0010337
Product name: 3,5-Bis(methoxycarbonyl)benzoicacid
Purity: 97.60%
Packaging: 1g
Price: $405
Updated: 2021/12/16

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1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER Chemical Properties,Usage,Production

Synthesis

2672-58-4

38588-64-6

18263-95-1

Trimethyl 1,3,5-benzenetricarboxylic acid ester (62 g, 246 mmol) was used as raw material and dissolved in a mixed solution of methanol (800 mL) and water. Aqueous sodium hydroxide solution (221 mL, 221 mmol, 1 N) was added slowly under vigorous stirring. The suspension was gradually dissolved over a period of 8 hours. The reaction mixture was continued to be stirred at room temperature for 18 hours. Subsequently, the solvent was removed by vacuum distillation. Dichloromethane (600 mL) was added to the remaining solid and the organic phase was washed with saturated aqueous sodium bicarbonate. The organic layer was separated through a partition funnel and washed three times with sodium bicarbonate solution (3 x 500 mL). After filtration, the solids were rinsed with a funnel. The crude product was analyzed by LC-MS and the molecular weight was confirmed as the target product 3,5-bis(methoxycarbonyl)benzoic acid (MW: 238; 48.8 g; 83% yield). The material in the organic layer was analyzed by LC-MS as a mixture of the target product and the over-hydrolysis product 5-(methoxycarbonyl)isophthalic acid (MW: 224; 9 g), and the material in the aqueous layer was analyzed as the starting material.

References

[1] Patent: US2016/24159, 2016, A1. Location in patent: Paragraph 1043-1044
[2] Chemical Communications, 2006, # 42, p. 4404 - 4406

1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER Suppliers

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38588-64-6, 1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTERRelated Search:

TRIS-[11-PENTAKIS-(4'-ETHYLPHENYLETHYNYL)PHENOXYUNDECYL]TRIMESATE TRIMETHYL 1,3,5-BENZENETRICARBOXYLATE 1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER Triethyl 1,3,5-benzenetricarboxylate BENZENE-1,3,5-TRICARBOXCYLIC ACID TRIS-[4-[6-(4-PROPYL-PHENYLETHYNYL)NAPHTHALENE-2-YLOXY]BUTYL] ESTER RARECHEM AL BF 1185 4,4'-(2-ACETYL-1,3-GLYCEROL) BISANHYDRO MELLITATE TRIALLYL 1,3,5-BENZENETRICARBOXYLATE BENZENEHEXACARBOXYLIC ACID HEXAMETHYL ESTER MELLITIC TRIANHYDRIDE DIETHYL 1,3,5-BENZENETRICARBOXYLATE TRIS-[11-PENTAKIS-(4'-PROPYLPHENYLETHYNYL)PHENOXYUNDECYL]TRIMESATE

1,3,5-BENZENETRICARBOXYLIC ACID DIMETHYL ESTER

3,5-bis(Methoxycarbonyl)benzoic acid

1,3,5-Benzenetricarboxylic acid, 1,3-dimethyl ester

3,5-bis(methoxycarbonyl)benzoicaci

3,5-di(methoxycarbonyl)benzoic acid

38588-64-6

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